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Gulf Coast Conference 2018

Gulf Coast Conference 2018

Restek at GCC 2018
Restek at GCC 2018

ORAL SESSION

Wednesday, October 17
9:00 a.m.-12:00 p.m./Floral Hall A2
Petrochem GC Applications Workshop
Jeff Werner1, Jan Pijpelink2 (presenter)
1Shimadzu, 2Restek Corporation
For more information, email Jan Pijpelink.
Read abstract

Welcome to the RESTEK/SHIMADZU Petrochem GC Applications workshop. Because of the need for more accuracy in refinery environments, customers are asking for a closer look at existing analytical techniques. The industry is looking for different approaches to monitor their refining processes. ASTM, as the leading standardization body for this industry, is making changes to existing methods to meet the industry’s needs. We will also be covering several new and modified GC configurations for analysis, including the new Nexis GC-2030 from Shimadzu. Please, join us for what is sure to be an informative discussion.

This workshop will provide an overview of various Petroleum Applications using Gas Chromatography. Covered topics include System and Custom GCs as well as Petroleum Applications Trends and ASTM Developments.

#258 – ASTM DO2.D Committee Meeting: Committee on Hydrocarbons for Chemical and Special Uses
3:30 PM – 5:30 PM /Floral Hall A1
USER Group

SEMINAR

Tuesday, October 16
10:15 a.m.–10:45 a.m./Tulip Room
Techniques to speed up the analysis in gas chromatography
Katarina Oden (Presenter), Christopher Rattray, Jaap de Zeeuw, Keith Irwin
Restek Corporation
For more information, email Katarina Oden.
Read abstract

In this seminar, we will discuss options to reduce the analysis time in gas chromatography without major investment in equipment nor investment in time to redevelop existing methods.

Ways to speed up the analysis depends on the resolution between the components of interest. Whenever there is plenty of resolution between the compounds the analysis time can be decreased by simply shortening the column or increasing the flow rate. However, in cases where we do not have extra column efficiency, the options are to switch to a more efficient carrier gas or use shorter, narrow bore, thinner film columns. Regardless of the choice, to maintain the elution order between the compounds or preserve resolutions, the methods have to be properly translated.

Practical examples will demonstrate:

  1. Using Restek’s EZGC method translator to speeding up the analysis while scaling down to smaller, high-efficiency, narrow-bore columns.

  2. Presented will be a migration of ASTM D2887 simulated distillation from a slower procedure A to faster procedure B using a slow, 120V oven and the GC Accelerator kit. The GC Accelerator kit provides a simple way to speed up sample analysis. By reducing oven volume, these inserts allow faster ramp rates to be attained.

  3. Speeding up a DHA run by increasing the flow on a long, narrow bore column.

POSTER SESSIONS

Wednesday, October 17
10:00 a.m./South Lobby
#256 - Applicability of micro packed columns (1/16" x 1 mm id) packed with DiatoSorb solid support and configured for use in a dedicated capillary Agilent 6890 and 7890 GC
Barry Burger (presenter)
Restek Corporation
For more information, email Barry Burger.
Read abstract

Columns and packings made with DiatoSorb solid support are superior in performance and reproducibility because Restek is the only global supplier that completely controls the physical and chemical properties of chromatographic-grade diatomaceous earth. This poster will demonstrate the performance, inertness, and speed of analysis obtained using Sulfinert-coated stainless steel micro packed columns (1/16 inch OD x 1 mm ID) compared to traditional packed columns (1/8 inch OD x 2 mm ID). The micro packed columns are easily installed and configured for on-column injection in a dedicated capillary Agilent 6890 or 7890 capillary GC as well as in a standard packed column GC.

2:00 p.m./South Lobby
#258 - Solutions for analysis of FAME Biodiesel quality using gas chromatography
Katarina Oden (presenter), Barry Burger
Restek Corporation
For more information, email Katarina Oden.
Read abstract

Fatty Acids Methyl Ester (FAME) biodiesel is currently the most popular alternative fuel on the market. Biofuel burns cleaner and emits fewer greenhouse gases than traditional sources of energy. Therefore, it also makes for an environmentally friendlier option.

FAME biodiesel is made from animal or vegetable fats with transesterification using acidic or basic catalyst and alcohol. All the steps of the reactions are strictly monitored and the final product is evaluated for reaction yields, residual starting materials, and byproducts. Presented will be solutions for determination of the final FAME content, residual alcohols, and glycerol/glycerides using gas chromatography.

Check back often! More details and other presentations will be added soon.

Visit the Gulf Coast Conference website.

Restek at GCC 2018