Column:

Rxi™-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)

Sample:

SV Calibration Mix #5 / 610 PAH Mix (cat.# 31011)

Inj.:

1.0µL, 10ppm each analyte (10ng on column), splitless (hold 0.1 min.) 4mm Drilled Uniliner® inlet liner (hole at bottom) (cat.# 20771)

Instrument:

Agilent 6890

Inj. temp.:

275°C

Carrier gas:

helium, constant flow

Flow rate:

1.2mL/min.

Oven temp.:

75°C (hold 0.5 min.) to 245°C @ 25°C/min., to 330°C @ 4°C/min. (hold 1 min.)

Det.:

Agilent 5973 GC/MS

Transfer line temp.:

280°C

Scan range:

35-550 amu

Solvent delay:

2 min.

Tune:

DFTPP

Ionization:

EI