Derivatized Amphetamines (500 ng/mL) on Rxi®-5Sil MS
| Peaks |
| 1. | Amphetamine |
| 2. | Methamphetamine |
| Peaks |
|---|
| 3. | MDA |
| 4. | MDMA |
| 5. | MDEA |
c = contaminant
GC_CF1144
| Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
|
| Butyl chloride |
| 500 ng/mL HFAA derivatives |
|
| 1 µL splitless (hold 1 min.) |
| 3.5mm Gooseneck Splitless w/Wool (cat.# 22286-200.1) |
| 250 °C |
| 28 mL/min. |
|
| 75 °C to 300 °C at 15 °C/min. |
| He, constant linear velocity |
| 45 cm/sec., 13.5 psi, 93.1 kPa @ 75 °C |
| MS |
| Scan |
| 250 °C |
| Quadrupole |
| 200 °C |
| 70 eV |
| 4 min. |
| PFTBA |
| EI |
| 40-300 amu |
| 5 scans/sec. |
| Shimadzu 2010 GC & QP2010+ MS |
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