Rtx®-CLPesticides, 30 m, 0.32 mm ID, 0.32 µm (cat.# 11141)
Sample
PCB Kit #1 diluted to 1,000 ppb in hexane (cat.# 32089)
decachlorobiphenyl (BZ #209) diluted to 100 ppb in acetone (cat.# 32029)
Injection
Inj. Vol.:
1.0 µL pulsed splitless (hold 0.3 min)
Liner:
Cyclo Double Gooseneck (4mm) (cat.# 20895)
Inj. Temp.:
250 °C
Pulse Pressure:
30 psi (206.8kPa)
Oven
Oven Temp:
120 °C to 200 °C at 45 °C/min to 230 °C at 15 °C/min to 330 °C at 30 °C/min (hold 2 min)
Carrier Gas
He, constant flow
Linear Velocity:
60 cm/sec
Detector
μ-ECD @ 330 °C
Notes
This chromatogram was obtained using an Agilent μ-ECD. To obtain comparable results, you will need to employ a μ-ECD in addition to confirmational dual-columns connected to a 5-meter guard column using a “Y” Press-Tight® connector.
