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Florida TRPH Standard on Rxi-5HT (15 m x 0.25 mm x 0.10 µm)

Florida TRPH Standard on Rxi®-5HT (15 m x 0.25 mm x 0.10 µm)

PeakstR (sec)
1.C864.1
2.C10124.9
3.C12203.5
4.C14279.7
5.C16349.0
6.C18411.5
7.C20468.7
8.C22521.1
PeakstR (sec)
9.C24569.3
10.C26613.9
11.C28655.4
12.C30694.3
13.C32730.6
14.C34764.8
15.C36797.0
16.C38827.5
17.C40856.7
image
GC_EV1377
ColumnRxi®-5HT, 15 m, 0.25 mm ID, 0.10 µm (cat.# 13905)
SampleFlorida TRPH standard (cat.# 31266)
Diluent:Hexane
Conc.:500 ng/µL
Injection
Inj. Vol.:1 µL split (split ratio 250:1)
Liner:Premium 4 mm Precision liner w/wool (cat.# 23305.5)
Inj. Temp.:275 °C
Split Vent Flow Rate:437.5 mL/min
Oven
Oven Temp.:40 °C (hold 0.1 min) to 400 °C at 19.6 °C/min (hold 1.53 min)
Carrier GasH2, constant flow
Flow Rate:1.75 mL/min
DetectorFID @ 420 °C
Constant Column + Constant Make-up:50 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:20 Hz
InstrumentAgilent/HP6890 GC
NotesActual column length was calculated to be 15.7 m using holdup time and EZGC® flow calculator (http://www.restek.com/ezgc-mtfc).
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