Pure Chromatography
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Nonylphenol, Bisphenol A, 4-tert-Octylphenol, Nonylphenol Monoethoxylate, and Nonylphenol Diethoxylate on Rxi®-XLB by ASTM D7065-11
Peaks 3, 6, and 9 correspond to mixtures of isomers.

GC_EV1404
Column | Rxi®-XLB, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13723) | ||||||||
Sample | Method 525.2 internal standard mix (cat.# 31825) | ||||||||
AccuStandard® nonylphenol calibration standard (cat.# M-1626) | |||||||||
Diluent: | Dichloromethane | ||||||||
Conc.: | See peak table for individual compound concentrations and amounts on-column. | ||||||||
Injection | |||||||||
Inj. Vol.: | 1 µL split (split ratio 10:1) | ||||||||
Liner: | Premium 4 mm Precision® liner w/wool (cat.# 23305.5) | ||||||||
Inj. Temp.: | 250 °C | ||||||||
Oven | |||||||||
Oven Temp.: | 45 °C (hold 1 min) to 305 °C at 8 °C/min (hold 1 min) | ||||||||
Carrier Gas | He, constant flow | ||||||||
Flow Rate: | 1.4 mL/min | ||||||||
Detector | MS | ||||||||
Mode: | Scan | ||||||||
Scan Program: |
| ||||||||
Transfer Line Temp.: | 300 °C | ||||||||
Analyzer Type: | Quadrupole | ||||||||
Source Type: | CI | ||||||||
Source Temp.: | 300 °C | ||||||||
Quad Temp.: | 150 °C | ||||||||
Ionization Mode: | EI | ||||||||
Instrument | Agilent 7890B GC & 5977A MSD |
RELATED CHROMATOGRAM LIBRARY SEARCHES
nonylphenols
,branched nonylphenol monoethoxylate
,branched nonylphenol diethoxylate
,NP
,NP1EO
,NP2EO
,OP
,BPA
,Bisphenol A
,surfactants
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