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Cannabinoids on Rxi-35Sil MS Using Hydrogen Carrier Gas by GC-FID

Cannabinoids on Rxi®-35Sil MS Using Hydrogen Carrier Gas by GC-FID

PeakstR (sec)
1.Cannabichromene83.3
2.Cannabidiol85.9
3.Delta-8-Tetrahydrocannabinol94.9
PeakstR (sec)
4.Delta-9-Tetrahydrocannabinol98.4
5.Cannabigerol100.9
6.Cannabinol106.7
image
GC_FS0501
ColumnRxi®-35Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 13820)
SampleCannabinoids standard (cat.# 34014)
Cannabichromene (cat.# 34092)
delta-8-Tetrahydrocannabinol (THC) (cat.# 34090)
Cannabigerol (cat.# 34091)
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4 mm Precision® liner w/wool (cat.# 23305.5)
Inj. Temp.:250 °C
Split Vent Flow Rate:125 mL/min
Oven
Oven Temp.:225 °C (hold 0.1 min) to 330 °C at 35 °C/min (hold 0.9 min)
Carrier GasH2, constant flow
Flow Rate:2.5 mL/min
DetectorFID @ 350 °C
Constant Column + Constant Make-up:50 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:20 Hz
InstrumentAgilent/HP6890 GC
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