Fast Detailed Hydrocarbons Analysis (DHA) on Rtx®-DHA-100 / Rtx®-5 DHA

Peaks
1.Ethanol
2.C5
3.tert-Butanol
4.2-Methylbutene-2
image
GC_PC00774A
ColumnRtx®-DHA-100, 100 m, 0.25 mm ID, 0.50 µm (cat.# 10148)
using Rtx®-5 DHA tuning column 5 m, 0.25 mm ID,
Samplefront slice of DHA/oxygenates setup blend
Injection
Inj. Vol.:0.01 µL split (split ratio 150:1)
Liner:Cup Splitter with Siltek® Deactivation (cat.# 20709-214.1)
Inj. Temp.:250 °C
Oven
Oven Temp:35 °C
Carrier GasH2, constant flow
Flow Rate:3.62 mL/min
Linear Velocity:55 cm/sec
DetectorFID @ 300 °C
NotesFront end of DHA/oxygenates setup blend
C5 efficiency: 586,825 plates
C5 k’: 0.476
tert-butanol skew: 2.10
Resolution tert-butanol/
2-methylbutene-2: 5.39
AcknowledgementChromatogram courtesy of Neil Johansen, Inc., Aztec, New Mexico, in association with Envantage Analytical Software, Inc., Cleveland, Ohio.
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