Carbamates on Ultra Carbamate
| Peaks |
| 1. | Aldicarb sulfone |
| 2. | Aldicarb sulfoxide |
| 3. | Oxamyl |
| 4. | Methomyl |
| 5. | 3-Hydroxycarbofuran |
| Peaks |
|---|
| 6. | Aldicarb |
| 7. | Propoxur |
| 8. | Carbofurane |
| 9. | Carbaryl |
| 10. | Methiocarb |
| 11. | BDMC (IS) |
LC_FF0473
| Ultra Carbamate (cat.# 9177352) |
| 50 mm x 2.1 mm ID |
| 3 µm |
| 100 Å |
|
| ambient |
| 531.1 Carbamate Pesticide Calibration Mixture (cat.# 32273) |
| 4-bromo-3,5-dimethylphenyl-N-methylcarbamate (BDMC) (cat.# 32274) |
| methanol |
| 50 µg/mL |
| 1 µL |
|
| 2mM ammonium acetate:methanol (v/v, 90/10) |
| 2mM ammonium acetate:methanol (v/v, 10/90) |
| | Time (min) | %A | %B |
|---|
| 0 | 80 | 20 | | 20 | 0 | 100 | | 25 | 0 | 100 |
|
| 0.2 mL/min |
| LECO Unique® TOFMS |
| 25 min |
| high flow ESI |
| positive |
| 130 °C |
| 100 kPa |
| 4 L/min |
| 120 °C |
| 62 V |
| 2.75 kV |
| Agilent 1100 |
| LECO Corporation |
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