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Pesticides on Ultra Aqueous C18

Pesticides on Ultra Aqueous C18

PeakstR (min)Transition 1Transition 2
1.Acrinathrin9.09540 -> 372540 -> 299.9
2.Chlorfluazuron9.24539.9 -> 356.8539.9 -> 519.7
3.Clothianidin3.63249.9 -> 58247.9 -> 59
4.Diflubenzuron7.68309 -> 156.1310 -> 288.9
5.Diuron6.78230.9 -> 185.8230.9 -> 149.8
6.Fluazinam7.99462.5 -> 415.8462.5 -> 397.9
7.Fludioxonil6.93246.9 -> 179.9246.9 -> 125.9
8.Forchlorfenuron6.44246 -> 126.9246 -> 91.2
9.Hexaflumuron8.45459 -> 438.8459 -> 174.9
10.Imibenconazol8.82409 -> 250.9411 -> 253
11.Lufenuron8.87509 -> 325.9509 -> 175
12.Metaflumizon8.5505.1 -> 301.9505.1 -> 140.9
13.Metamitron3.97201 -> 184.8201 -> 116.9
14.Methoxyfenozid6.98366.9 -> 104.9366.9 -> 148.9
15.Nitenpyram2.59269.2 -> 221.6269.2 -> 100.8
16.Novaluron8.42491.1 -> 470.7493.1 -> 472.7
17.Profoxydim7.57464.3 -> 277.9464.3 -> 126.8
18.Propoxycarbazon3.09396.9 -> 156396.9 -> 112.9
19.Prothioconazol7.16342 -> 100.1343.9 -> 99.9
20.Tebufenozid7.46350.9 -> 149350.9 -> 105
21.Teflubenzuron8.85378.6 -> 338.8378.6 -> 195.9
22.Tepraloxydim4.57340 -> 248340 -> 220.1
23.Terbacil5.38214.9 -> 158.9216.9 -> 160.9
24.Tralkoxydim6.28328.1 -> 253.8328.1 -> 281.8
25.Triadimefon7.01292 -> 67.9292 -> 234.9
26.Triflumuron8356.9 -> 153.8358.9 -> 155.9
image
LC_FF0490A
ColumnUltra Aqueous C18 (cat.# 9178312)
Dimensions:100 mm x 2.1 mm ID
Particle Size:3 µm
Pore Size:100 Å
Temp.:35 °C
Samplemulticomponent pesticide standard
Diluent:water
Conc.:1 ppb each pesticide
Inj. Vol.:10 µL
Mobile Phase
A:10 mM NH4OAc in water
B:10 mM NH4OAc in methanol
Time (min)%B
0.0020
8.090
12.0100
14.8100
14.920
Flow:0.5 mL/min
DetectorApplied Biosystems/MDS Sciex LC/MS/MS
Model #:4000 QTRAP®
Ion Source:TurboIonSpray®
Ion Mode:ESI-
Ion Spray Voltage:-4.2 kV
Gas 1:50 psi (344.7 kPa)
Gas 2:60 psi (413.7 kPa)
Source Temp.:600 °C
InstrumentShimadzu UFLCXR
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