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NJ Low Level TO-15 75 Component Mix on Rtx-VMS (60 m, 40 °C start)
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NJ Low Level TO-15 75 Component Mix on Rtx-VMS (60 m, 40 °C start)
Peaks tR (min)
1. Propylene 3.45
2. Dichlorodifluoromethane (Freon 12) 3.54
3. 1,2-Dichlorotetrafluoroethane (Freon 114) 3.82
4. Chloromethane 3.94
5. n- Butane4.00
6. Vinyl chloride 4.11
7. 1,3-Butadiene 4.15
8. Bromomethane 4.81
9. Chloroethane 5.09
10. Vinyl bromide 5.35
11. n- Pentane5.39
12. Trichlorofluoromethane (Freon 11) 5.40
13. 1,1-Dichloroethene 6.58
14. Ethanol 6.61
15. Carbon disulfide 6.63
16. 1,1,2-Trichlorotrifluoroethane (Freon 113) 6.69
17. Acrolein 7.45
18. Allyl chloride 7.68
19. Isopropyl alcohol 7.87
20. Methylene chloride 7.87
21. Acetone 8.03
22. trans- 1,2-Dichloroethene8.13
23. Hexane 8.25
24. Methyl tert- butyl ether (MTBE) 8.37
25. Tertiary butanol 8.58
26. 1,1-Dichloroethane 9.01
27. Vinyl acetate 9.32
28. cis- 1,2-Dichloroethene9.63
29. Cyclohexane 9.82
30. Bromochloromethane (IS) 9.84
31. Chloroform 9.90
32. Carbon tetrachloride 10.03
33. Ethyl acetate 10.04
34. 1,1,1-Trichloroethane 10.10
35. Tetrahydrofuran 10.10
36. 2-Butanone (MEK) 10.23
37. Isooctane 10.29
38. Heptane 10.37
39. Benzene 10.44
Peaks tR (min)
40. 1,2-Dichloroethane 10.62
41. Trichloroethylene 10.91
42. 1,4-Difluorobenzene (IS) 10.93
43. 1,2-Dichloropropane 11.32
44. Bromodichloromethane 11.35
45. Methyl methacrylate 11.44
46. 1,4-Dioxane 11.51
47. cis- 1,3-Dichloropropene11.78
48. Toluene 11.93
49. 4-Methyl-2-pentanone (MIBK) 12.17
50. Tetrachloroethene 12.18
51. trans- 1,3-Dichloropropene12.18
52. 1,1,2-Trichloroethane 12.30
53. Dibromochloromethane 12.42
54. 1,2-Dibromoethane 12.59
55. 2-Hexanone (MBK) 12.67
56. n- Nonane12.74
57. Ethylbenzene 12.87
58. Chlorobenzene-d5 (IS) 12.88
59. Chlorobenzene 12.89
60. m- Xylene12.95
61. p- Xylene12.95
62. o- Xylene13.21
63. Styrene 13.24
64. Bromoform 13.30
65. Cumene 13.38
66. 4-Bromofluorobenzene* 13.57
67. n- Propyl benzene13.61
68. 1,1,2,2-Tetrachloroethane 13.65
69. 4-Ethyltoluene 13.66
70. 1,3,5-Trimethylbenzene 13.69
71. 2-Chlorotoluene 13.73
72. 1,2,4-Trimethylbenzene 13.93
73. 1,3-Dichlorobenzene 14.16
74. 1,4-Dichlorobenzene 14.21
75. Benzyl chloride 14.34
76. 1,2-Dichlorobenzene 14.46
77. Hexachlorobutadiene 15.29
78. 1,2,4-Trichlorobenzene 15.35
79. Naphthalene 15.60
*Tuning standard
GC_AR1167
Rtx-VMS, 60 m, 0.25 mm ID, 1.40 µm (cat.# 19916) with MXT low-dead-volume connector kit (cat.# 20536) TO-14A internal standard/tuning mix (cat.# 34408) 75 comp TO15 + NJ mix (cat.# 34396)
Air @ 50% RH 5 ppbv 250 mL injection on-column 40 °C (hold 7 min) to 250 °C at 30 °C/min (hold 2 min) He, constant flow 2.0 mL/min MS Scan Group Start Time (min) Scan Range (amu) Scan Rate (scans/sec) 1 0.00 35.0 - 226.00 3.8
250 °C Quadrupole Extractor 6 mm ID 230 °C 150 °C 70.0 eV BFB EI Markes CIA Advantage Agilent 7890B GC & 5977A MSD
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