share:
delim
delim
Extracted Opiates from Blood on Rxi-5Sil MS
This chromatogram may contain analytes that are synonyms of your search terms.

Extracted Opiates from Blood on Rxi-5Sil MS

Peaks
1.Hydrocodone
2.Codeine
3.Oxycodone
4.Hydromorphone
5.6-Monoacetylmorphine
6.Morphine
* Matrix
image
GC_CF1150
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Sample
Diluent:Ethyl acetate
Conc.:100 ng/mL propionic anhydride derivatives
Injection
Inj. Vol.:1 µL splitless (hold 1 min)
Liner:4 mm splitless taper w/wool (cat.# 22405)
Inj. Temp.:250 °C
Purge Flow:100 mL/min
Oven
Oven Temp.:65 °C (hold 1 min) to 315 °C at 15 °C/min
Carrier GasHe, constant flow
Flow Rate:1 mL/min
Linear Velocity:35 cm/sec @ 65 °C
DetectorMS
Mode:SIM
Transfer Line Temp.:250 °C
Analyzer Type:Quadrupole
Solvent Delay Time:7 min
Tune Type:PFTBA
Ionization Mode:EI
NotesOpiates were spiked into a blood sample and extracted by SPE, then derivatized with propionic anhydride.
AcknowledgementData courtesy of Miami Dade County Medical Examiner Department
Download PDF

RELATED CHROMATOGRAM LIBRARY SEARCHES

Opiates

,

Rxi

,

Rxi-5SilMS

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us