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Comparison of Single Taper Liners with Wool for Amphetamine Peak Shape

Comparison of Single Taper Liners with Wool for Amphetamine Peak Shape

Peaks
1.Amphetamine
image
GC_CF1151
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Sampleamphetamine
Diluent:1-chlorobutane
Conc.:~10 µg/mL
Injection
Inj. Vol.:1 µL splitless (hold 1 min)
Liner:Comparison of Premium Single Taper with Wool (cat.# 23303.5) and SGE Single Taper with Wool (cat.# 092019)
Inj. Temp.:250 °C
Purge Flow:20 mL/min
Oven
Oven Temp.:45 °C to 250 °C at 20 °C/min
Carrier GasHe, constant flow
Flow Rate:2 mL/min
DetectorFID @ 350 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
InstrumentAgilent 7890A GC
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