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Phenols & Benzidines US EPA Methods 604 & 605 on Rtx-5

Phenols & Benzidines US EPA Methods 604 & 605 on Rtx-5

Peaks
1.Phenol
2.2-Chlorophenol
3.2-Nitrophenol
4.2,4-Dimethylphenol
5.2,4-Dichlorophenol
6.4-Chloro-3-methylphenol
Peaks
7.2,4,6-Trichlorophenol
8.2,4-Dinitrophenol
9.4-Nitrophenol
10.2-Methyl-4,6-dinitrophenol
11.Pentachlorophenol
12.Benzidine
13.3,3'-Dichlorobenzidine
image
GC_EV00033
ColumnRtx-5, 30 m, 0.53 mm ID, 1.50 µm (cat.# 10270)
Sample604 Phenols Calibration Mix (cat.# 31029)
605 Benzidines Calibration Mix (cat.# 31030)
Conc.: concentration approximately 25ng per component
Injection
Inj. Vol.:2.5 µL splitless
Inj. Temp.:300 °C
Oven
Oven Temp.:40 °C (hold 6 min) to 300 °C at 10 °C/min (hold 15 min)
Carrier GasH2, constant linear velocity
Linear Velocity:80 cm/sec
DetectorFID @ 300 °C
NotesFlow rate: 10 cc/min
FID sensitivity: 8 x 10-11 AFS
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