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Alaska Method AK101AA on Rtx-5Sil MS (FID)

Alaska Method AK101AA on Rtx-5Sil MS (FID)

Peaks
1.Hexane
2.Benzene
3.α,α,α-Trifluorotoluene (SS)
4.Toluene
5.Ethylbenzene
6.m-Xylene
7.p-Xylene
8.o-Xylene
9.Isopropylbenzene
Peaks
10.4-Bromofluorobenzene (SS)
11.n-Propylbenzene
12.1-Ethyl-3-methylbenzene
13.1-Ethyl-4-methylbenzene
14.1,3,5-Trimethylbenzene
15.1-Ethyl-2-methylbenzene
16.1,2,4-Trimethylbenzene
17.Decane
18.1,2,3-Trimethylbenzene
image
GC_EV00402
ColumnRtx-5Sil MS, 40 m, 0.45 mm ID, 1.50 µm (cat.# 12798)
Sample4-bromofluorobenzene (cat.# 30026)
α,α,α-trifluorotoluene (cat.# 30048)
Alaska UST Method AK101AA, Ver. 3-1-99 (cat.# 30461)
Diluent:5mL RO water
Conc.:10 ppb
Injectionpurge and trap splitless
Purge and Trap
Instrument:Tekmar LSC3000 Purge and Trap
Trap Type:BTEX Trap
Interface Connection:direct
Transfer Line Tubing:Siltek transfer line
Oven
Oven Temp.:40 °C (hold 2 min) to 85 °C at 4 °C/min (hold 1 min) to 225 °C at 40 °C/min (hold 2 min)
DetectorFID @ 280 °C
Make-up Gas Flow Rate:15 mL/min
NotesInstrument: Finnigan 9001
see also: Alaska Method AK101AA on Rtx-5Sil MS (PID) GC_EV00402
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