share:
delim
delim
Volatile Organics by EPA Method 8260 (80ppb Standard) on Rtx-VMS

Volatile Organics by EPA Method 8260 (80ppb Standard) on Rtx-VMS

Peaks
1.Dichlorodifluoromethane
2.Chloromethane
3.Vinyl chloride
4.Bromomethane
5.Chloroethane
6.Trichlorofluoromethane
7.Diethyl ether
8.1,1-Dichloroethene
9.Carbon disulfide
10.1,1,2-Trichloro-1,2,2-trifluoroethane
11.Iodomethane
12.Allyl chloride
13.Methylene chloride
14.Acetone
15.trans-1,2-Dichloroethene
16.Methyl-D3-tert-butyl-ether
17.Methyl acetate
18.Methyl tert-butyl ether
19.tert-Butyl alcohol
20.Acetonitrile
21.Diisopropyl ether
22.Chloroprene
23.1,1-Dichloroethane
24.Acrylonitrile
25.Ethyl tert-butyl ether
26.cis-1,2-Dichloroethene
27.2,2-Dichloropropane
28.Bromochloromethane
29.Chloroform
30.Carbon tetrachloride
31.Tetrahydrofuran
32.Methyl acrylate
33.1,1,1-Trichloroethane
34.Dibromofluoromethane
35.1,1-Dichloropropene
36.2-Butanone
37.Benzene
38.Propionitrile
39.Methacrylonitrile
40.1,2-Dichloroethane-D4
41.Pentafluorobenzene
42.tert-Amyl methyl ether
43.1,2-Dichloroethane
44.Isobutyl alcohol
45.Trichloroethene
46.1,4-Difluorobenzene
47.Dibromomethane
48.1,2-Dichloropropane
49.Bromodichloromethane
50.Methyl methacrylate
51.cis-1,3-Dichloropropene
Peaks
52.2-Chloroethyl vinyl ether
53.Toluene-d8
54.Toluene
55.2-Nitropropane
56.Tetrachloroethene
57.2-Bromo-1-chloropropane
58.4-Methyl-2-pentanone
59.trans-1,3-Dichloropropene
60.1,1,2-Trichloroethane
61.Ethyl methacrylate
62.Dibromochloromethane
63.1,3-Dichloropropane
64.1,2-Dibromoethane
65.2-Hexanone
66.Chlorobenzene-D5
67.Chlorobenzene
68.Ethylbenzene
69.1,1,1,2-Tetrachloroethane
70.m-Xylene
71.p-Xylene
72.o-Xylene
73.Bromoform
74.Styrene
75.Isopropylbenzene
76.4-Bromo-1-fluorobenzene
77.Bromobenzene
78.cis-1,4-Dichloro-2-butene
79.1,4-Dichlorobutane
80.n-Propylbenzene
81.1,1,2,2-Tetrachloroethane
82.2-Chlorotoluene
83.1,2,3-Trichloropropane
84.1,3,5-Trimethylbenzene
85.trans-1,4-Dichloro-2-butene
86.4-Chlorotoluene
87.tert-Butylbenzene
88.Pentachloroethane
89.1,2,4-Trimethylbenzene
90.sec-Butylbenzene
91.p-Isopropyltoluene
92.1,3-Dichlorobenzene
93.1,4-Dichlorobenzene-D4
94.1,4-Dichlorobenzene
95.n-Butylbenzene
96.1,2-Dichlorobenzene
97.1,2-Dibromo-3-chloropropane
98.Nitrobenzene
99.Hexachlorobutadiene
100.1,2,4-Trichlorobenzene
101.Naphthalene
102.1,2,3-Trichlorobenzene
*Carbon dioxide
image
GC_EV00685
ColumnRtx-VMS, 30 m, 0.25 mm ID, 1.4 µm (cat.# 19915)
Sample8260B MegaMix calibration mix kit (cat.# 30475)
California oxygenates mix (cat.# 30465)
VOA calibration mix #1 (ketones) (cat.# 30006)
8260A surrogate mix (cat.# 30240)
8260 internal standard mix (cat.# 30074)
Injectionpurge and trap split (split ratio 25:1)
Inj. Temp.:250 °C
Purge and Trap
Instrument:O.I. Analytical 4560 with 4551A Autosampler
Trap Type:#10 (Tenax/silica gel/carbon molecular sieve)
Purge: 11 min @ 20 °C, flow 38 mL/min
Desorb Preheat Temp.:150 °C
Desorb: 1.0 min @ 190 °C, flow 32 mL/min
Bake: 10 min @ 210 °C
Transfer Line Temp.:110 °C
Oven
Oven Temp.:35 °C (hold 7 min) to 90 °C at 4 °C/min to 220 °C at 45 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.3 mL/min
Dead Time:1.47 min @ 35 °C
DetectorAgilent 5971A GC-MS
Transfer Line Temp.:280 °C
Tune Type:PFTBA/BFB
Scan Range:35-260 amu
NotesSample Size: 10 mL
Sample Temp: 40 °C
Water Management: 110 °C purge, 0 °C desorb, 240 °C bake
6-Port Valve: 110 °C
Sparge Mount: 45 °C
Valve Manifold: 50 °C
Other Conditions: prepurge, preheat, dry purge OFF
AcknowledgementPurge & trap courtesy of O.I. Analytical
Download PDF

RELATED CHROMATOGRAM LIBRARY SEARCHES

xylene

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.