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Polycyclic Aromatic Hydrocarbons by EPA Method 610 on Rxi-5ms

Polycyclic Aromatic Hydrocarbons by EPA Method 610 on Rxi-5ms

Peaks
1.Naphthalene
2.Acenaphthylene
3.Acenaphthene
4.Fluorene
5.Phenanthrene
6.Anthracene
7.Fluoranthene
8.Pyrene
Peaks
9.Benz[a]anthracene
10.Chrysene
11.Benzo[b]fluoranthene
12.Benzo[k]fluoranthene
13.Benzo[a]pyrene
14.Indeno[1,2,3-cd]pyrene
15.Dibenz[a,h]anthracene
16.Benzo[ghi]perylene
image
GC_EV00824
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleSV Calibration Mix #5 / 610 PAH Mix (cat.# 31011)
Conc.:10 ppm each analyte (10 ng on-column)
Injection
Inj. Vol.:1.0 µL splitless (hold 0.1 min)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:275 °C
Oven
Oven Temp.:75 °C (hold 0.5 min) to 245 °C at 25 °C/min to 330 °C at 4 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Solvent Delay Time:2 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
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polynuclear aromatic hydrocarbons

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polycyclic aromatic hydrocarbons

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