Pure Chromatography
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Polycyclic Aromatic Hydrocarbons by EPA Method 610 on Rxi-5ms
| Peaks | |
|---|---|
| 1. | Naphthalene |
| 2. | Acenaphthylene |
| 3. | Acenaphthene |
| 4. | Fluorene |
| 5. | Phenanthrene |
| 6. | Anthracene |
| 7. | Fluoranthene |
| 8. | Pyrene |
| Peaks | |
|---|---|
| 9. | Benz[a]anthracene |
| 10. | Chrysene |
| 11. | Benzo[b]fluoranthene |
| 12. | Benzo[k]fluoranthene |
| 13. | Benzo[a]pyrene |
| 14. | Indeno[1,2,3-cd]pyrene |
| 15. | Dibenz[a,h]anthracene |
| 16. | Benzo[ghi]perylene |
GC_EV00824
| Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) |
| Sample | SV Calibration Mix #5 / 610 PAH Mix (cat.# 31011) |
| Conc.: | 10 ppm each analyte (10 ng on-column) |
| Injection | |
| Inj. Vol.: | 1.0 µL splitless (hold 0.1 min) |
| Liner: | Drilled Uniliner (hole near bottom) (cat.# 20771) |
| Inj. Temp.: | 275 °C |
| Oven | |
| Oven Temp.: | 75 °C (hold 0.5 min) to 245 °C at 25 °C/min to 330 °C at 4 °C/min (hold 1 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1.2 mL/min |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 280 °C |
| Analyzer Type: | Quadrupole |
| Solvent Delay Time: | 2 min |
| Tune Type: | DFTPP |
| Ionization Mode: | EI |
| Scan Range: | 35-550 amu |
| Instrument | HP6890 GC & 5973 MSD |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2019 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.