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Polycyclic Aromatic Hydrocarbons by EPA 610 on Rxi-5ms

Polycyclic Aromatic Hydrocarbons by EPA 610 on Rxi-5ms

Peaks
1.2-Fluorophenol
2.Phenol-d6-
3.1,4-Dichlorobenzene-d4
4.Nitrobenzene-d5
5.Naphthalene-d8
6.Naphthalene
7.2-Fluorobiphenyl
8.Acenaphthylene
9.Acenaphthene-d10
10.Acenaphthene
11.Fluorene
12.2,4,6-Tribromophenol
13.Phenanthrene-d10
14.Phenanthrene
Peaks
15.Anthracene
16.Fluoranthene
17.Pyrene
18.p-Terphenyl-d14
19.Benz[a]anthracene
20.Chrysene-d12
21.Chrysene
22.Benzo[b]fluoranthene
23.Benzo[k]fluoranthene
24.Benzo[a]pyrene
25.Perylene-d12
26.Indeno[1,2,3-cd]pyrene
27.Dibenz[a,h]anthracene
28.Benzo[ghi]perylene
image
GC_EV00825
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleSV Calibration Mix #5 / 610 PAH Mix (cat.# 31011)
Acid Surrogate Mix (4/89 SOW) (cat.# 31025)
B/N Surrogate Mix (4/89 SOW) (cat.# 31024)
SV Internal Standard Mix (cat.# 31206)
Conc.: 10 ng/µL each analyte, 40 ng/μL internal standards
Injection
Inj. Vol.:1.0 µL splitless (hold 0.1 min)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:275 °C
Oven
Oven Temp.:75 °C (hold 0.5 min) to 245 °C at 25 °C/min to 330 °C at 4 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Solvent Delay Time:2 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
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PAH

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polycyclic aromatic hydrocarbons

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polynuclear aromatic hydrocarbons

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