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Minnesota Dept. of Agriculture List 1 Pesticides on Rxi-1ms

Minnesota Dept. of Agriculture List 1 Pesticides on Rxi-1ms

Peaks
1.2-Fluorophenol (SS)
2.Phenol-d6 (SS)
3.1,4-Dichlorobenzene-d4 (IS)
4.Nitrobenzene-d5 (SS)
5.Naphthalene-d8 (IS)
6.EPTC
7.2-Fluorobiphenyl (SS)
8.Acenaphthene-d10 (IS)
9.Propachlor
10.Desisopropylatrazine
11.Desethyl-atrazine
12.2,4,6-Tribromophenol (SS)
13.Ethalfluralin
14.Trifluralin
15.Phorate
16.Simazine
17.Prometon
Peaks
18.Atrazine
19.Propazine
20.Terbufos
21.Fonofos
22.Phenanthrene-d10 (IS)
23.Triallate
24.Metribuzin
25.Dimethenamid
26.Acetochlor
27.Alachlor
28.Cyanazine
29.Metolachlor
30.Chlorpyrifos
31.Pendimethalin
32.p-Terphenyl-d14 (SS)
33.Chrysene-d12 (IS)
34.Perylene-d12 (IS)
image
GC_EV00837
ColumnRxi-1ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13323)
SampleMinnesota Ag List 1 Pesticides Mix A (cat.# 32406)
Minnesota Ag List 1 Pesticides Mix B (cat.# 32407)
SV Internal Standard Mix (cat.# 31206)
B/N Surrogate Mix (4/89 SOW) (cat.# 31024)
Acid Surrogate Mix (4/89 SOW) (cat.# 31025)
Conc.:10 µg/mL each analyte (internal standards 25ug/ml)
Injection
Inj. Vol.:1.0 µL split (split ratio 10:1)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:250 °C
Oven
Oven Temp.:70 °C (hold 1 min) to 180 °C at 20 °C/min to 230 °C at 5 °C/min to 325 °C at 40 °C/min (hold 3.5 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Solvent Delay Time:2.5 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
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