Pure Chromatography
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Organochlorine Pesticide Mix AB #2 Rtx-CLPesticides and Rtx-CLPesticides2 (0.25mm ID column set)
| Peaks | |
|---|---|
| 1. | 2,4,5,6-tetrachloro-m-xylene (SS) |
| 2. | α-BHC |
| 3. | γ-BHC |
| 4. | β-BHC |
| 5. | δ-BHC |
| 6. | Heptachlor |
| 7. | Aldrin |
| 8. | Heptachlor epoxide (isomer B) |
| 9. | trans-Chlordane* |
| 10. | cis-Chlordane* |
| 11. | Endosulfan I |
| Peaks | |
|---|---|
| 12. | 4,4'-DDE |
| 13. | Dieldrin |
| 14. | Endrin |
| 15. | 4,4'-DDD |
| 16. | Endosulfan II |
| 17. | 4,4'-DDT |
| 18. | Endrin aldehyde |
| 19. | Endosulfan sulfate |
| 20. | Methoxychlor |
| 21. | Endrin ketone |
| 22. | decachlorobiphenyl (SS) |
* For information regarding the nomenclature used for cis-chlordane and trans-chlordane, visit www.restek.com/chlordane-notice
GC_EV00941
| Columns | Rtx-CLPesticides 30 m, 0.25 mm ID, 0.25 µm (cat.# 11123) |
| and Rtx-CLPesticides2 30 m, 0.25 mm ID, 0.20 µm (cat.# 11323) | |
| using Rxi guard column 5 m, 0.25 mm ID (cat.# 10029) | |
| with Siltek-treated universal “Y” Press-Tight connector (cat.# 20486) | |
| Sample | Organochlorine pesticide mix AB #2 (cat.# 32292) |
| Pesticide surrogate mix, EPA 8080, 8081 (cat.# 32000) | |
| Injection | |
| Inj. Vol.: | 0.5 µL splitless (hold 0.5 min) |
| Liner: | Cyclo double taper (2 mm) (cat.# 20908) |
| Inj. Temp.: | 250 °C |
| Oven | |
| Oven Temp.: | 125 °C to 200 °C at 45 °C/min to 230 °C at 12.5 °C/min to 330 °C at 30 °C/min (hold 2 min) |
| Carrier Gas | He, constant linear velocity |
| Linear Velocity: | 41 cm/sec @ 125 °C |
| Detector | ECD @ 330 °C |
| Notes | This chromatogram was obtained using an Agilent μ-ECD. To obtain comparable results, you will need to employ a μ-ECD in addition to dual columns connected to a 5-meter guard column using a “Y” Press-Tight connector. |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2019 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.