Semivolatiles by EPA Method 8270 on Rxi-5Sil MS (30m, 0.25mm ID, 0.50µm)

	Peaks
1.	1,4-Dioxane
2.	N-Nitrosodimethylamine
3.	Pyridine
4.	2-Fluorophenol (SS)
5.	Phenol-d6- (SS)
6.	Phenol
7.	Aniline
8.	Bis(2-chloroethyl) ether
9.	2-Chlorophenol
10.	1,3-Dichlorobenzene
11.	1,4-dichlorobenzene-d4 (IS)
12.	1,4-Dichlorobenzene
13.	Benzyl alcohol
14.	2-Methylphenol
15.	1,2-Dichlorobenzene
16.	Bis(2-chloroisopropyl) ether
17.	4-methylphenol/3-methylphenol
18.	N-Nitrosodi-N-propylamine
19.	Hexachloroethane
20.	nitrobenzene-d5 (SS)
21.	Nitrobenzene
22.	Isophorone
23.	2,4-Dimethylphenol
24.	Benzoic acid
25.	2-Nitrophenol
26.	Bis(2-chloroethoxy)methane
27.	2,4-Dichlorophenol
28.	1,2,4-Trichlorobenzene
29.	Naphthalene-d8 (IS)
30.	Naphthalene
31.	4-Chloroaniline
32.	Hexachlorobutadiene
33.	4-Chloro-3-methylphenol
34.	2-Methylnaphthalene
35.	1-Methylnaphthalene
36.	Hexachlorocyclopentadiene
37.	2,4,6-Trichlorophenol
38.	2,4,5-Trichlorophenol
39.	2-Fluorobiphenyl (SS)
40.	2-Chloronaphthalene
41.	2-Nitroaniline
42.	1,4-Dinitrobenzene
43.	Dimethyl phthalate
44.	1,3-Dinitrobenzene
45.	2,6-Dinitrotoluene
46.	1,2-Dinitrobenzene

	Peaks
47.	Acenaphthylene
48.	3-Nitroaniline
49.	acenaphthene-d10 (IS)
50.	2,4-Dinitrophenol
51.	Acenaphthene
52.	4-Nitrophenol
53.	2,4-Dinitrotoluene
54.	Dibenzofuran
55.	2,3,5,6-Tetrachlorophenol
56.	2,3,4,6-Tetrachlorophenol
57.	Diethyl phthalate
58.	4-Chlorophenyl phenyl ether
59.	4-Nitroanaline
60.	Fluorene
61.	4,6-Dinitro-2-methylphenol
62.	n-Nitroso-diphenylamine (diphenylamine
63.	1,2-Diphenylhydrazine (as azobenzene)
64.	2,4,6-Tribromophenol (SS)
65.	4-Bromophenyl phenyl ether
66.	Hexachlorobenzene
67.	Pentachlorophenol
68.	Phenanthrene-d10 (IS)
69.	Phenanthrene
70.	Anthracene
71.	Carbazole
72.	di-n-Butyl phthalate
73.	Fluoranthene
74.	Benzidine
75.	Pyrene-d10 (SS)
76.	3,3'-Dimethylbenzidine
77.	Pyrene
78.	p-terphenyl-d14 (SS)
79.	Butyl benzyl phthalate
80.	Bis(2-ethylhexyl) adipate
81.	Bis(2-ethylhexyl)phthalate
82.	3,3'-Dichlorobenzidine
83.	Benzo[a]anthracene
84.	Chrysene-d12 (IS)
85.	Chrysene
86.	Di-n-octyl phthalate
87.	Benzo[b]fluoranthene
88.	Benzo[k]fluoranthene
89.	Benz[a]pyrene
90.	Perylene-d12 (IS)
91.	Dibenzo[a,h]anthracene
92.	Indeno[1,2,3-cd]pyrene
93.	Benzo[ghi]perylene

GC_EV00944

Column	Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.50 µm (cat.# 13638)
Sample	8270 MegaMix (cat.# 31850)
	benzoic acid (cat.# 31879)
	8270 Benzidines Mix (cat.# 31852)
	Acid Surrogate Mix (4/89 SOW) (cat.# 31025)
	Revised B/N Surrogate Mix (cat.# 31887)
	1,4-Dioxane (cat.# 31853)
	SV Internal Standard Mix (cat.# 31206)
Conc.:	10 ng on-column concentration
Injection
Inj. Vol.:	1.0 µL pulsed splitless (hold 0.25 min)
Liner:	Drilled Uniliner (hole near bottom) (cat.# 20756)
Inj. Temp.:	250 °C
Pulse Pressure:	30 psi (206.8kPa)
Pulse Time:	0.3 min
Purge Flow:	40 mL/min
Oven
Oven Temp.:	40 °C (hold 1.0 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 3.5 min)
Carrier Gas	He, constant flow
Flow Rate:	1.2 mL/min
Detector	MS
Mode:	Scan
Transfer Line Temp.:	280 °C
Ionization Mode:	EI
Scan Range:	35-550 amu

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Recommendations

	8270 MegaMix Standard cat.# 31850 Qty:
	Benzoic Acid cat.# 31879 Qty:
	8270 Benzidines Mix cat.# 31852 Qty:
	Acid Surrogate Mix (4/89 SOW) cat.# 31025 Qty:
	Revised B/N Surrogate Mix cat.# 31887 Qty:
	1,4-Dioxane cat.# 31853 Qty:
	SV Internal Standard Mix cat.# 31206 Qty:
	Rxi-5Sil MS Columns cat.# 13638 Qty:

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Semivolatiles by EPA Method 8270 on Rxi-5Sil MS (30m, 0.25mm ID, 0.50µm)

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