Pure Chromatography
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Brominated Flame Retardants on Rtx-1614
Peaks | |
---|---|
1. | BDE-10![]() |
2. | BDE-7![]() |
3. | BDE-8![]() |
4. | BDE-11![]() |
5. | BDE-12![]() |
6. | BDE-13![]() |
7. | BDE-15![]() |
8. | BDE-30![]() |
9. | BDE-32![]() |
10. | BDE-17![]() |
11. | BDE-25![]() |
12. | BDE-28![]() |
13. | BDE-33![]() |
Peaks | |
---|---|
14. | BDE-35![]() |
15. | BDE-37![]() |
16. | BDE-75![]() |
17. | BDE-49![]() |
18. | BDE-71![]() |
19. | BDE-47![]() |
20. | BDE-66![]() |
21. | BDE-77![]() |
22. | BDE-100![]() |
23. | BDE-119![]() |
24. | BDE-99![]() |
25. | BDE-116![]() |
26. | BDE-118![]() |
27. | BDE-85![]() |
Peaks | |
---|---|
28. | BDE-155![]() |
29. | BDE-126![]() |
30. | BDE-154![]() |
31. | BDE-153![]() |
32. | BDE-138![]() |
33. | BDE-166![]() |
34. | BDE-183![]() |
35. | BDE-181![]() |
36. | BDE-190![]() |
37. | BDE-208![]() |
38. | BDE-207![]() |
39. | BDE-206![]() |
40. | BDE-209![]() |

GC_EV01025
Column | Rtx-1614, 15 m, 0.25 mm ID, 0.10 µm (cat.# 10296) |
Sample | 100-300 ppb PBDE PAR solution (#EO-5113, Cambridge Isotope Laboratories Inc.) |
500 ppb decabromodiphenyl ether (#BDE-209, Wellington Laboratories) | |
Injection | |
Inj. Vol.: | 1 µL splitless (hold 1 min) |
Liner: | 4 mm cyclo double taper (cat.# 20896) |
Inj. Temp.: | 340 °C |
Oven | |
Oven Temp.: | 120 °C (hold 1 min) to 275 °C at 15 °C/min to 300 °C at 5 °C/min (hold 5 min) |
Carrier Gas | He, constant linear velocity |
Linear Velocity: | 60 cm/sec @ 120 °C |
Detector | µ-ECD @ 345 °C |
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