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Comparison of Single Taper Liners with Wool for 2,4-DNP Recovery

Comparison of Single Taper Liners with Wool for 2,4-DNP Recovery

Peaks
1.Acenaphthene (IS)
2.2,4-DNP
image
GC_EV1204
ColumnRxi-5Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 13620)
Sample2,4-dinitrophenol and acenaphthene standard
Diluent:methylene chloride
Conc.:10 µg/mL each
Injection
Inj. Vol.:1 µL splitless (hold 1 min)
Liner:Comparison of Premium Single Taper Inlet Liner with Wool (cat.# 23303.5) and Non-Premium Single Taper Inlet Liner with Wool
Inj. Temp.:250 °C
Purge Flow:20 mL/min
Oven
Oven Temp.:50 °C to 150 °C at 20 °C/min (hold 2.2 min)
Carrier GasHe, constant flow
Flow Rate:1.5 mL/min
DetectorFID @ 300 °C
Make-up Gas Flow Rate:30 mL/min
Make-up Gas Type:N2
InstrumentAgilent/HP6890 GC
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