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PAHs and PCB Congeners on Rxi-XLB

PAHs and PCB Congeners on Rxi-XLB

PeaksConc.
(µg/mL)
1.Naphthalene5
2.2-Methylnaphthalene5
3.Acenaphthylene5
4.Acenaphthene5
5.Fluorene5
6.Phenanthrene5
7.Anthracene5
8.PCB 311
9.PCB 281
10.PCB 521
11.Fluoranthene5
12.PCB 1011
13.Pyrene5
14.2-Methylfluoranthene5
PeaksConc.
(µg/mL)
15.PCB 1181
16.PCB 1531
17.PCB 1381
18.PCB 1801
19.Benzo[a]anthracene5
20.Chrysene5
21.Triphenylene5
22.PCB 1941
23.Benzo[b]fluoranthene5
24.Benzo[k]fluoranthene5
25.Benzo[e]pyrene5
26.Benzo[a]pyrene5
27.Dibenzo[a,h]anthracene5
28.Indeno[1,2,3-cd]pyrene5
29.Benzo[ghi]perylene5
image
GC_EV1223
ColumnRxi-XLB, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13723)
SampleSV calibration mix #5 / 610 PAH mix (cat.# 31011)
Benzo(e)pyrene (cat.# custom)
Triphenylene (cat.# custom)
2-Methylnaphthalene (cat.# 31285)
2-Methylfluoranthene (cat.# custom)
PCB congener standard #2 (cat.# 32294)
PCB 31 (cat.# custom)
Diluent:Dichloromethane
Injection
Inj. Vol.:0.5 µL splitless (hold 1.75 min)
Liner:2.0 mm ID straight inlet liner w/wool (cat.# 21718)
Inj. Temp.:300 °C
Purge Flow:50 mL/min
Oven
Oven Temp.:40 °C (hold 2 min) to 240 °C at 30 °C/min (hold 2 min) to 340 °C at 10 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Temp.:280 °C
Electron Energy:70 eV
Solvent Delay Time:4 min
Tune Type:manual
Ionization Mode:EI
Scan Range:45-550 amu
Scan Rate:5 scans/sec
InstrumentPE Clarus 500 GC & Clarus 500 MS
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XLB

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