share:
delim
delim
PCBs and BFRs on Rxi-XLB and Rxi-17Sil MS (GCxGC)

PCBs and BFRs on Rxi-XLB and Rxi-17Sil MS (GCxGC)

image
GC_EV1237
ColumnRxi-XLB 30 m, 0.25 mm ID, 0.25 µm (cat.# 13723)
Rxi-17Sil MS 1 m, 0.15 mm ID, 0.15 µm (cat.# 43820)
  with IP deactivated guard column 0.2 m, 0.15 mm ID
SamplePBDE mix (cat.# 33098)
PCB congener mix, Method 8082A (cat.# 32416)
Diluent:Isooctane
Conc.:250 pg/µL
Injection
Inj. Vol.:1.0 µL splitless (hold 1.0 min)
Liner:Premium 4 mm single taper w/wool (cat.# 23303.5)
Inj. Temp.:250 °C
Purge Flow:20 mL/min
Oven
Oven Temp.:Rxi-XLB: 80 °C (hold 1 min) to 120 °C at 10 °C/min to 300 °C at 3 °C/min
Rxi-17Sil MS: 85 °C (hold 1 min) to 125 °C at 10 °C/min to 305 °C at 3 °C/min
Carrier GasHe, corrected constant flow (2.0 mL/min)
Modulation
Modulator Temp. Offset:20 °C
Second Dimension Separation Time:3.5 sec
Hot Pulse Time:1.25 sec
Cool Time between Stages:0.50 sec
Detectorµ-ECD @ 325 °C
Data Rate:50 Hz
InstrumentAgilent/HP6890 GC
NotesThe Rxi-17Sil MS column (cat.# 43820) is a 10 m column. A 1 m section was used as a second dimension column.
Guard column was connected using a Siltek-treated universal Press-Tight connector (cat.# 20480).
Download PDF

RELATED CHROMATOGRAM LIBRARY SEARCHES

brominated diphenyl ether

,

Brominated flame retardant

,

PBDE

,

PCB

,

polychlorinated biphenyl

,

BDE

,

BFR

,

GCxGC

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us