Pure Chromatography
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EU PCB Congeners on Rxi-XLB
| Peaks | |
|---|---|
| 1. | PCB 31 |
| 2. | PCB 28 |
| 3. | PCB 52 |
| 4. | PCB 101 |
| 5. | PCB 118 |
| 6. | PCB 153 |
| 7. | PCB 138 |
| 8. | PCB 180 |
| 9. | PCB 194 |
GC_EV1240
| Column | Rxi-XLB, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13723) |
| Sample | PCB congener standard #2 (cat.# 32294) |
| PCB 31 (cat.# custom) | |
| Diluent: | Dichloromethane |
| Conc.: | 3.5 ppm |
| Injection | |
| Inj. Vol.: | 0.5 µL splitless (hold 1.75 min) |
| Liner: | 2.0 mm ID straight inlet liner w/wool (cat.# 21718) |
| Inj. Temp.: | 300 °C |
| Purge Flow: | 50 mL/min |
| Oven | |
| Oven Temp.: | 40 °C (hold 2 min) to 240 °C at 30 °C/min (hold 2 min) to 340 °C at 10 °C/min (hold 5 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1 mL/min |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 300 °C |
| Analyzer Type: | Quadrupole |
| Source Temp.: | 280 °C |
| Electron Energy: | 70 eV |
| Ionization Mode: | EI |
| Scan Range: | 45-550 amu |
| Scan Rate: | 5 scans/sec |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2020 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.