Pure Chromatography
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Tetrachlorofurans on Rtx-Dioxin2 (60 m x 0.18 mm x 0.10 µm)
GC_EV1301
| Column | Rtx-Dioxin2, 60 m, 0.18 mm ID, 0.10 µm (cat.# custom) |
| Sample | Fly ash extract |
| Diluent: | Nonane |
| Conc.: | This is a "real world" sample extract. |
| Injection | |
| Inj. Vol.: | 1 µL splitless (hold 1 min) |
| Liner: | Premium 2 mm single taper w/wool (cat.# 23316.1) |
| Inj. Temp.: | 280 °C |
| Purge Flow: | 40 mL/min |
| Oven | |
| Oven Temp.: | 120 °C (hold 1 min) to 200 °C at 35 °C/min to 280 °C at 4.5 °C/min to 330 °C at 20 °C/min (hold 4.8 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1 mL/min |
| Detector | HRMS |
| Mode: | Scan |
| Transfer Line Temp.: | 300 °C |
| Analyzer Type: | Magnetic Sector |
| Source Temp.: | 280 °C |
| Tune Type: | PFK |
| Electron Energy: | 40 eV |
| Resolving Power: | 10,000 |
| Instrument | Waters AutoSpec Ultima Mass Spectrometer |
| Acknowledgement | Terry Kolic, Ontario Ministry of Environment |
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