Pure Chromatography
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Semivolatiles With Appendix IX on Rxi-5ms by 8270D
| Peaks | |
|---|---|
| 1. | 1,4-Dioxane-d8 (IS)  |
| 2. | 1,4-Dioxane |
| 3. | N-Nitrosodimethylamine |
| 4. | Pyridine |
| 5. | Ethyl methacrylate |
| 6. | 2-Picoline |
| 7. | N-Nitrosomethylethylamine |
| 8. | Methyl methanesulfonate |
| 9. | 2-Fluorophenol (SS) |
| 10. | N-Nitrosodiethylamine |
| 11. | Ethyl methanesulfonate |
| 12. | Benzaldehyde |
| 13. | Phenol-d6 (SS) |
| 14. | Phenol |
| 15. | Aniline |
| 16. | Pentachloroethane |
| 17. | Bis(2-chloroethyl) ether |
| 18. | 2-Chlorophenol |
| 19. | 1,3-Dichlorobenzene |
| 20. | 1,4-Dichlorobenzene-d4 (IS) |
| 21. | 1,4-Dichlorobenzene |
| 22. | Benzyl alcohol |
| 23. | 1,2-Dichlorobenzene |
| 24. | 2-Methylphenol |
| 25. | Bis(2-Chloroisopropyl)ether |
| 26. | p-Cresol (4-methylphenol) |
| 27. | m-Cresol (3-methylphenol) |
| 28. | N-Nitrosopyrrolidine |
| 29. | Acetophenone |
| 30. | N-Nitrosodi-n-propylamine |
| 31. | 4-Nitrosomorpholine |
| 32. | o-Toluidine |
| 33. | Hexachloroethane |
| 34. | Nitrobenzene-d5 (SS) |
| 35. | Nitrobenzene |
| 36. | N-Nitrosopiperidine |
| 37. | Isophorone |
| 38. | 2-Nitrophenol |
| 39. | 2,4-Dimethylphenol |
| 40. | Benzoic acid |
| 41. | Bis(2-chloroethoxy)methane |
| 42. | 2,4-Dichlorophenol |
| 43. | α,α-Dimethylphenethylamine (Phentermine) |
| 44. | 1,2,4-Trichlorobenzene |
| 45. | Naphthalene-d8 (IS) |
| 46. | Naphthalene |
| 47. | 4-Chloroaniline |
| 48. | 2,6-Dichlorophenol |
| 49. | Hexachloropropene |
| 50. | Hexachlorobutadiene |
| 51. | Caprolactam |
| 52. | N-Nitroso-N-butylamine |
| 53. | 1,4-Phenylenediamine |
| 54. | 4-Chloro-3-methylphenol |
| 55. | Isosafrole I (isomer) |
| 56. | 2-Methylnaphthalene |
| 57. | 1-Methylnaphthalene |
| 58. | Isosafrole II (isomer) |
| 59. | 1,2,4,5-Tetrachlorobenzene |
| 60. | Hexachlorocyclopentadiene |
| 61. | 2,4,6-Trichlorophenol |
| 62. | 2,4,5-Trichlorophenol |
| 63. | 2-Fluorobiphenyl (SS) |
| 64. | Safrole |
| 65. | Biphenyl |
| 66. | 2-Chloronaphthalene |
| 67. | 1-Chloronaphthalene |
| 68. | Diphenyl ether |
| 69. | 2-Nitroaniline |
| 70. | 1,4-Naphthoquinone |
| 71. | 1,4-Dinitrobenzene |
| 72. | Dimethyl phthalate |
| Peaks | |
|---|---|
| 73. | 1,3-Dinitrobenzene |
| 74. | 2,6-Dinitrotoluene |
| 75. | Acenaphthylene |
| 76. | 1,2-Dinitrobenzene |
| 77. | 3-Nitroaniline |
| 78. | Acenaphthene-d10 (IS) |
| 79. | Acenaphthene |
| 80. | 2,4-Dinitrophenol |
| 81. | 4-Nitrophenol |
| 82. | Dibenzofuran |
| 83. | 2,4-Dinitrotoluene |
| 84. | Pentachlorobenzene |
| 85. | 1-Naphthalamine |
| 86. | 2,3,5,6-Tetrachlorophenol |
| 87. | 2-Naphthalamine |
| 88. | 2,3,4,6-Tetrachlorophenol |
| 89. | Diethyl phthalate |
| 90. | 4-Chlorophenyl phenyl ether |
| 91. | Fluorene |
| 92. | 2-Methyl-5-nitroaniline |
| 93. | 4-Nitroaniline |
| 94. | 4,6-Dinitro-2-methylphenol |
| 95. | N-Nitrosodiphenylamine |
| 96. | 1,2-Diphenylhydrazine (as Azobenzene) |
| 97. | 2,4,6-Tribromophenol (SS) |
| 98. | 1,3,5-Trinitrobenzene |
| 99. | Diallate |
| 100. | Phenacetin |
| 101. | 4-Bromophenyl phenyl ether |
| 102. | Hexachlorobenzene |
| 103. | Atrazine |
| 104. | 4-Aminobiphenyl |
| 105. | Pentachlorophenol |
| 106. | Propyzamide |
| 107. | Pentachloronitrobenzene |
| 108. | Phenanthrene-d10 (IS) |
| 109. | Phenanthrene |
| 110. | Anthracene |
| 111. | Carbazole |
| 112. | di-n-Butyl phthalate |
| 113. | 4-Nitroquinoline oxide |
| 114. | Isodrin |
| 115. | Fluoranthene |
| 116. | Benzidine |
| 117. | Pyrene-d10 (SS) |
| 118. | Pyrene |
| 119. | Aramite I (isomer) |
| 120. | p-Terphenyl-d14 (SS) |
| 121. | Aramite II (isomer) |
| 122. | Dimethylaminoazobenzene |
| 123. | Chlorobenzilate |
| 124. | 3,3'-Dimethylbenzidine |
| 125. | Butyl benzyl phthalate |
| 126. | Kepone |
| 127. | Bis(2-ethylhexyl) adipate |
| 128. | 2-Acetylaminofluorine |
| 129. | 3,3'-Dichlorobenzidine |
| 130. | Benz[a]anthracene |
| 131. | Chrysene-d12 (IS) |
| 132. | Chrysene |
| 133. | Bis(2-ethylhexyl) phthalate |
| 134. | Di-n-octyl phthalate |
| 135. | Benzo[b]fluoranthene |
| 136. | 7,12-Dimethylbenzo[a]anthracene |
| 137. | Benzo[k]fluoranthene |
| 138. | Benzo[a]pyrene |
| 139. | Perylene-d12 (IS) |
| 140. | 3-Methylcholanthrene |
| 141. | Dibenz[a,j]acridine |
| 142. | Indeno[1,2,3-cd]pyrene |
| 143. | Dibenz[a,h]anthracene |
| 144. | Benzo[ghi]perylene |
GC_EV1304
| Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) | ||||||||
| Sample | Revised SV internal standard mix (cat.# 31886) | ||||||||
| Revised B/N surrogate mix (cat.# 31888) | |||||||||
| Acid surrogate mix (4/89 SOW) (cat.# 31063) | |||||||||
| 8270 MegaMix (cat.# 31850) | |||||||||
| 8270 Benzidines mix (cat.# 31852) | |||||||||
| Benzoic acid (cat.# 31879) | |||||||||
| Appendix IX mix #1, revised (cat.# 32459) | |||||||||
| Appendix IX mix #2 (cat.# 31806) | |||||||||
| Diluent: | Dichloromethane | ||||||||
| Conc.: | 10 µg/mL (IS/SS 20 µg/mL) | ||||||||
| Injection | |||||||||
| Inj. Vol.: | 1 µL split (split ratio 10:1) | ||||||||
| Liner: | Premium 4 mm Precision liner w/wool (cat.# 23305.5) | ||||||||
| Inj. Temp.: | 275 °C | ||||||||
| Split Vent Flow Rate: | 14.4 mL/min | ||||||||
| Oven | |||||||||
| Oven Temp.: | 50 °C (hold 0.5 min) to 265 °C at 28 °C/min to 285 °C at 3 °C/min to 330 °C at 25 °C/min (hold 1 min) | ||||||||
| Carrier Gas | He, constant flow | ||||||||
| Flow Rate: | 1.44 mL/min | ||||||||
| Detector | MS | ||||||||
| Mode: | Scan | ||||||||
| Scan Program: |
| ||||||||
| Transfer Line Temp.: | 290 °C | ||||||||
| Analyzer Type: | Quadrupole | ||||||||
| Source Temp.: | 330 °C | ||||||||
| Quad Temp.: | 180 °C | ||||||||
| Electron Energy: | 70 eV | ||||||||
| Solvent Delay Time: | 1.35 min | ||||||||
| Tune Type: | DFTPP | ||||||||
| Ionization Mode: | EI | ||||||||
| Instrument | Agilent 7890A GC & 5975C MSD |
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Copyright © 2021 Restek Corporation. All rights reserved.
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Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.