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Brominated Flame Retardants on Rtx-1614 After Two Loops Were Trimmed Off

GC_EV1306
Column | Rtx-1614, 14.4 m, 0.25 mm ID, 0.10 µm (cat.# 10296) |
Sample | Native PBDEs/BFRs (Wellington Laboratories) (cat.# BFR-PAR) |
Diluent: | Nonane/toluene |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 1.0 min) |
Liner: | Premium 4 mm cyclo double taper (cat.# 23310.5) |
Inj. Temp.: | 340 °C |
Oven | |
Oven Temp.: | 75 °C (hold 0.9 min) to 210 °C at 21 °C/min to 310 °C at 9 °C/min (hold 3.6 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.6 mL/min |
Detector | MS |
Mode: | SIM |
Transfer Line Temp.: | 330 °C |
Analyzer Type: | Quadrupole |
Source Temp.: | 350 °C |
Quad Temp.: | 200 °C |
Instrument | Agilent 7890A GC & 5975C MSD |
Notes | Cat.# 10296 is a 15 m column. Two loops were trimmed off the column for a final column length of 14.4 m. |
RELATED CHROMATOGRAM LIBRARY SEARCHES
flame retardants
,column trimming
,Rtx-1614
,polybrominated diphenyl ethers
,PBDE
,BDE
,EPA Method 1614
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