Pure Chromatography
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Detailed Analysis of Polycyclic Aromatic Hydrocarbons (PAHs) in Creosote Oil on Rxi-PAH
| Peaks | |
|---|---|
| 1. | Benzo[ghi]fluoranthene |
| 2. | Benzo[c]phenanthrene |
| 3. | Benz[a]anthracene |
| 4. | Triphenylene |
| 5. | Chrysene |
| 6. | Benzo[b]fluoranthene |
| 7. | Benzo[k]fluoranthene |
| 8. | Benzo[j]fluoranthene |
| 9. | Benzo(a)fluoranthene |
| 10. | Benzo[e]pyrene |
| 11. | Benzo[a]pyrene |
| 12. | Perylene |
| Peaks | |
|---|---|
| 13. | Dibenzo(a,j)anthracene |
| 14. | Dibenz[a,c]anthracene |
| 15. | Indeno[1,2,3-cd]pyrene |
| 16. | Dibenz[a,h]anthracene |
| 17. | Benzo[b]chrysene |
| 18. | Picene |
| 19. | Benzo[ghi]perylene |
| 20. | Anthanthrene |
| 21. | Dibenzo[a,l]pyrene |
| 22. | Dibenzo[a,e]pyrene |
| 23. | Coronene |
| 24. | Dibenzo[a,i]pyrene |
| 25. | Dibenzo[a,h]pyrene |
GC_EV1391
| Column | Rxi-PAH, 60 m, 0.25 mm ID, 0.10 µm (cat.# 49317) | ||||||||||||
| Sample | Creosote oil standard (cat.# 31838) | ||||||||||||
| Diluent: | Dichloromethane | ||||||||||||
| Conc.: | 50,000 µg/mL | ||||||||||||
| Injection | |||||||||||||
| Inj. Vol.: | 1 µL split (split ratio 40:1) | ||||||||||||
| Liner: | Premium 4 mm Precision liner w/wool (cat.# 23305.5) | ||||||||||||
| Inj. Temp.: | 275 °C | ||||||||||||
| Split Vent Flow Rate: | 78 mL/min | ||||||||||||
| Oven | |||||||||||||
| Oven Temp.: | 40 °C (hold 1.6 min) to 210 °C at 24 °C/min to 295 °C at 1.9 °C/min to 350 °C at 3.7 °C/min (hold 6 min) | ||||||||||||
| Carrier Gas | He, constant flow | ||||||||||||
| Flow Rate: | 1.95 mL/min | ||||||||||||
| Detector | MS | ||||||||||||
| Mode: | Scan | ||||||||||||
| Scan Program: |
| ||||||||||||
| Transfer Line Temp.: | 330 °C | ||||||||||||
| Analyzer Type: | Quadrupole | ||||||||||||
| Source Type: | Extractor | ||||||||||||
| Extractor Lens: | 9mm ID | ||||||||||||
| Source Temp.: | 350 °C | ||||||||||||
| Quad Temp.: | 200 °C | ||||||||||||
| Electron Energy: | 70 eV | ||||||||||||
| Solvent Delay Time: | 3.4 min | ||||||||||||
| Instrument | Agilent 7890B GC & 5977A MSD |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2019 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.