Pure Chromatography
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Detailed Analysis of Polycyclic Aromatic Hydrocarbons (PAHs) in Creosote Oil on Rxi-PAH

GC_EV1391
Column | Rxi-PAH, 60 m, 0.25 mm ID, 0.10 µm (cat.# 49317) | ||||||||||||
Sample | Creosote oil standard (cat.# 31838) | ||||||||||||
Diluent: | Dichloromethane | ||||||||||||
Conc.: | 50,000 µg/mL | ||||||||||||
Injection | |||||||||||||
Inj. Vol.: | 1 µL split (split ratio 40:1) | ||||||||||||
Liner: | Premium 4 mm Precision liner w/wool (cat.# 23305.5) | ||||||||||||
Inj. Temp.: | 275 °C | ||||||||||||
Split Vent Flow Rate: | 78 mL/min | ||||||||||||
Oven | |||||||||||||
Oven Temp.: | 40 °C (hold 1.6 min) to 210 °C at 24 °C/min to 295 °C at 1.9 °C/min to 350 °C at 3.7 °C/min (hold 6 min) | ||||||||||||
Carrier Gas | He, constant flow | ||||||||||||
Flow Rate: | 1.95 mL/min | ||||||||||||
Detector | MS | ||||||||||||
Mode: | Scan | ||||||||||||
Scan Program: |
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Transfer Line Temp.: | 330 °C | ||||||||||||
Analyzer Type: | Quadrupole | ||||||||||||
Source Type: | Extractor | ||||||||||||
Extractor Lens: | 9mm ID | ||||||||||||
Source Temp.: | 350 °C | ||||||||||||
Quad Temp.: | 200 °C | ||||||||||||
Electron Energy: | 70 eV | ||||||||||||
Solvent Delay Time: | 3.4 min | ||||||||||||
Instrument | Agilent 7890B GC & 5977A MSD |
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