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NIST SRM 1975, Diesel Particulate Extract, on Rxi-PAH

This chromatogram may contain analytes that are synonyms of your search terms.

NIST SRM 1975, Diesel Particulate Extract, on Rxi-PAH

	Peaks
1.	Naphthalene-D8
2.	Naphthalene
3.	2-Methylnaphthalene
4.	Biphenyl
5.	Acenaphthylene
6.	Acenaphthene-D10
7.	Acenaphthene
8.	Fluorene
9.	Dibenzothiophene
10.	Phenanthrene-D10
11.	Phenanthrene
12.	Anthracene
13.	4H-Cyclopenta[def]phenanthrene
14.	Fluoranthene
15.	Pyrene
16.	Benzo[ghi]fluoranthene
17.	Benzo[c]phenanthrene
18.	Benz[a]anthracene
19.	Chrysene-D12

	Peaks
20.	Triphenylene
21.	Chrysene
22.	Benzo[b]fluoranthene
23.	Benzo[k]fluoranthene
24.	Benzo[j]fluoranthene
25.	Benzo[e]pyrene
26.	Benzo[a]pyrene-D12
27.	Benzo[a]pyrene
28.	Perylene-D12
29.	Dibenzo[a,j]anthracene
30.	Dibenzo[a,c]anthracene
31.	Indeno[1,2,3-cd]pyrene
32.	Dibenz[a,h]anthracene
33.	Benzo[b]chrysene
34.	Picene
35.	Benzo[ghi]perylene
36.	Dibenzo[b,k]fluoranthene
37.	Coronene-D12
38.	Coronene

GC_EV1392

Column

Rxi-PAH, 60 m, 0.25 mm ID, 0.10 µm (cat.# 49317)

Sample

NIST SRM 1975

Diluent:

Dichloromethane

Injection

Inj. Vol.:

1 µL split (split ratio 10:1)

Liner:

Premium 4 mm Precision liner w/wool (cat.# 23305.1)

Inj. Temp.:

275 °C

Split Vent Flow Rate:

19.5 mL/min

Oven

Oven Temp.:

110 °C (hold 1.6 min) to 210 °C at 24 °C/min to 295 °C at 1.9 °C/min to 350 °C at 3.7 °C/min (hold 6 min)

Carrier Gas

He, constant flow

Flow Rate:

1.95 mL/min

Detector

Mode:

SIM

SIM Program:

Group	Start Time (min)	Ion(s) (m/z)	Dwell (ms)
1	3.09	102.1, 108.1, 128.1, 136.2	40
2	5.69	115.1, 142.1	40
3	6.23	76.1, 141.1, 154.1, 156.2	40
4	6.95	75.6, 76.1, 91.1, 152.1, 153.1, 155.1, 162.2, 170.2	20
5	7.93	82.4, 165.1	40
6	9.19	139.1, 152.1, 160.2, 178.1, 184.1, 188.2	40
7	11.78	94.6, 165.1, 190.1, 192.1	40
8	14.19	101.1, 202.1	40
9	16.60	101.1, 202.1	40
10	18.49	92.1, 184.1	40
11	19.58	108, 216	40
12	22.3	196.1, 212.2	40
13	24.92	113.1, 226.1, 228.1	40
14	26.27	113.1, 114.0, 120.1, 226.1, 228.1, 240.1	40
15	28.75	154.1, 252.1	35
16	30.62	119.8, 242.2	40
17	35.29	126.1, 252.1	40
18	38.56	125.1, 252.1	40
19	39.23	126.1, 252.1	40
20	40.71	125.1, 126.1, 132.1, 252.1, 264.1	40
21	42.91	125, 132.2, 252.1, 264.1	40
22	44.35	252.1, 268.1	40
23	48.41	139.1, 139.5, 278.1, 279.1	40
24	52.13	139.1, 139.5, 278.1, 279.1	40
25	53.70	138.1, 139.1, 278.1	40
26	54.97	138.1, 276.1	40
27	55.92	138.1, 276.1	40
28	57.04	132.6, 267.1	40
29	59.69	151.0, 302.1	40
30	63.27	150, 151, 156.1, 300.1, 302.1, 312.1	40
31	64.78	151.0, 302.1	40

Transfer Line Temp.:

330 °C

Analyzer Type:

Quadrupole

Source Type:

Extractor

Extractor Lens:

9 mm ID

Source Temp.:

350 °C

Quad Temp.:

200 °C

Solvent Delay Time:

3 min

Tune Type:

DFTPP

Ionization Mode:

Instrument

Agilent 7890B GC & 5977A MSD

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NIST SRM 1975, Diesel Particulate Extract, on Rxi-PAH

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