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NJ DEP EPH Aromatics on Rxi-5Sil MS by Split Injection

GC_EV1489
Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
Sample | NJ DEP EPH 10/08 rev. 2 aromatics calibration standard (cat.# 30541) |
MA fractionation surrogate spike mix (cat.# 31480) | |
Diluent: | Methylene chloride |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 10:1) |
Liner: | Topaz 4 mm ID Precision inlet liner w/ wool (cat.# 23305) |
Inj. Temp.: | 300 °C |
Oven | |
Oven Temp.: | 55 °C (hold 0.5 min) to 150 °C at 20 °C/min to 250 °C at 30 °C/min to 280 °C at 5 °C/min to 345 °C at 30 °C/min (hold 3 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 4 mL/min |
Detector | FID @ 340 °C |
Make-up Gas Flow Rate: | 45 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 50 Hz |
Instrument | Agilent 7890A GC |
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