share:
delim
delim
GCxGC-TOFMS Contour Plot Showing Potential Isobaric Interference with Acephate (m/z 136) in 1D Analysis
This chromatogram may contain analytes that are synonyms of your search terms.

GCxGC-TOFMS Contour Plot Showing Potential Isobaric Interference with Acephate (m/z 136) in 1D Analysis

image
GC_FS0504
ColumnRxi-5ms 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
  with Rxi guard column 1.0 m, 0.25 mm ID (cat.# 10029)
Rtx-200 1.0 m, 0.25 mm ID, 0.25 µm (cat.# 15124)
Sample505 Organohalide pesticide mix (cat.# 32024)
QuEChERS performance standards kit (cat.# 31152)
QuEChERS internal standard mix for GC-MS analysis (cat.# 33267)
Diluent:Acetonitrile
Injection
Inj. Vol.:1.0 µL splitless (hold 1.0 min)
Liner:Premium 4 mm single taper (cat.# 23302.1)
Inj. Temp.:250 °C
Purge Flow:40 mL/min
Oven
Oven Temp.:Rxi-5ms: 70 °C (hold 1.0 min) to 330 °C at 8.0 °C/min (hold 6.5 min)
Rtx-200: 75 °C (hold 1.0 min) to 335 °C at 8.0 °C/min (hold 6.5 min)
Carrier GasHe, corrected constant flow (1.4 mL/min)
Modulation
Modulator Temp. Offset:20 °C
Second Dimension Separation Time:2.00 sec
Hot Pulse Time:0.60 sec
Cool Time between Stages:0.40 sec
DetectorMS
Mode:
Transfer Line Temp.:320 °C
Analyzer Type:TOF
Source Temp.:225 °C
Electron Energy:70 eV
Mass Defect:-20 mu/100 u
Ionization Mode:EI
Acquisition Range:45-550 amu
Spectral Acquisition Rate:100 spectra/sec
InstrumentLECO Pegasus 4D GCxGC-TOFMS
NotesAll column connections were made with an SGE SilTite µ-union.
Download PDF

RELATED CHROMATOGRAM LIBRARY SEARCHES

herbal tea

,

pesticides

,

GCxGC

,

QuEChERS

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us