Pure Chromatography
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Terpenes in Kryptonite Medical Cannabis on Rxi-624Sil MS
| Peaks | tR (sec) | |
|---|---|---|
| 1. | alpha-Pinene | 427.5 |
| 2. | Camphene | 446.2 |
| 3. | Myrcene | 465.7 |
| 4. | beta-Pinene | 470.0 |
| Peaks | tR (sec) | |
|---|---|---|
| 5. | Limonene | 506.6 |
| 6. | Linalool | 576.2 |
| 7. | Fenchone | 587.0 |
| 8. | alpha-Terpineol | 660.5 |
GC_FS0514
| Column | Rxi-624Sil MS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 13868) |
| Injection | |
| Inj. Vol.: | 1 µL split (split ratio 10:1) |
| Liner: | Premium 4 mm Precision w/wool (cat.# 23305.5) |
| Inj. Temp.: | 250 °C |
| Oven | |
| Oven Temp.: | 60 °C (hold 0.1 min) to 300 °C at 12.5 °C/min (hold 1.7 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1.4 mL/min |
| Detector | FID @ 320 °C |
| Constant Column + Constant Make-up: | 50 mL/min |
| Make-up Gas Type: | N2 |
| Hydrogen flow: | 40 mL/min |
| Air flow: | 450 mL/min |
| Data Rate: | 10 Hz |
| Instrument | Agilent/HP6890 GC |
| Notes | The sample was collected by blowing compressed air over medical cannabis and purging that air through methanol via an impinger setup. |
| Acknowledgement | Andrew Goldsmith - SRI Instruments |
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Copyright © 2019 Restek Corporation. All rights reserved.
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Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.