Pure Chromatography
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Cannabis Terpenes on Rxi-624Sil MS by FET-HS-GC

GC_FS0518
Column | Rxi-624Sil MS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 13868) |
Sample | Terpenes mix |
Diluent: | Isopropyl alcohol |
Conc.: | 200 ng/µL (0.02% wt/vol). The sample was prepared by placing 10 µL into the headspace vial. |
Injection | headspace-loop split (split ratio 10:1) |
Liner: | Premium 1.0 mm ID straight inlet liner (cat.# 23333.1) |
Headspace-Loop | |
Inj. Port Temp.: | 250 °C |
Instrument: | Tekmar HT-3 |
Inj. Time: | 1.0 min |
Transfer Line Temp.: | 160 °C |
Valve Oven Temp.: | 160 °C |
Needle Temp.: | 140 °C |
Sample Temp.: | 140 °C |
Sample Equil. Time: | 30.0 min |
Vial Pressure: | 20 psi |
Loop Pressure: | 15 psi |
Oven | |
Oven Temp.: | 60 °C (hold 0.10 min) to 300 °C at 12.50 °C/min (hold 3.0 min) |
Carrier Gas | He, constant flow |
Linear Velocity: | 33 cm/sec |
Detector | FID @ 320 °C |
Make-up Gas Flow Rate: | 45 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
Notes | For qualitative purposes only. |
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