Pure Chromatography
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GC Multiresidue Pesticide Standard #3-ONP on Rxi-5ms by GC-MS

GC_FS0602
Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) | ||||||||
Sample | GC multiresidue pesticide standard #3-ONP (cat.# 32565) | ||||||||
Diluent: | Toluene | ||||||||
Conc.: | 100 µg/mL | ||||||||
Injection | |||||||||
Inj. Vol.: | 1 µL split (split ratio 50:1) | ||||||||
Liner: | Premium 4.0 mm ID Precision inlet liner w/wool (cat.# 23305.1) | ||||||||
Inj. Temp.: | 250 °C | ||||||||
Oven | |||||||||
Oven Temp.: | 90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min) | ||||||||
Carrier Gas | He, constant flow | ||||||||
Flow Rate: | 1.4 mL/min | ||||||||
Detector | MS | ||||||||
Mode: | Scan | ||||||||
Scan Program: |
| ||||||||
Transfer Line Temp.: | 290 °C | ||||||||
Analyzer Type: | Quadrupole | ||||||||
Source Temp.: | 325 °C | ||||||||
Electron Energy: | 70 eV | ||||||||
Solvent Delay Time: | 5 min | ||||||||
Ionization Mode: | EI | ||||||||
Instrument | Thermo Scientific TSQ 8000 Triple Quadrupole GC-MS | ||||||||
Notes | Reconstructed chromatogram from select ions. |
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