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Ethylene and C1-C5 Hydrocarbons by ASTM D6159-97 on Rt-Alumina BOND/KCl, Rtx-1

Ethylene and C1-C5 Hydrocarbons by ASTM D6159-97 on Rt-Alumina BOND/KCl, Rtx-1

Peaks
1.Methane
2.Ethane
3.Ethylene
4.Propane
5.Cyclopropane
6.Propylene
7.Acetylene
8.Isobutane
9.Propadiene
Peaks
10.n-Butane
11.trans-2-Butene
12.1-Butene
13.Isobutylene
14.cis-2-Butene
15.iso-Pentane
16.Methylacetylene
17.n-Pentane
18.1,3-Butadiene
image
GC_PC01110
ColumnRt-Alumina BOND/KCl *, 50 m, 0.53 mm ID, 10 µm (cat.# 19760)
SampleEthylene gas plus C1 through C5 hydrocarbons
Injection
Inj. Vol.:1 µL split
Liner:2 mm splitless (cat.# 20712)
Inj. Temp.:200 °C
Split Vent Flow Rate:60 ml/min
Oven
Oven Temp.:35 °C (hold 2 min) to 190 °C at 4 °C/min (hold 15 min)
Carrier GasHe, constant pressure (8.0 psi, 55.2 kPa)
Linear Velocity:25.4 cm/sec @ 35 °C
DetectorFID @ 200 °C
Make-up Gas Type:N2
Data Rate:20 Hz
InstrumentHP5890 GC
Notes* Rt-Alumina BOND/KCl, 50 m, 0.53 mm ID, 10.0 μm (cat.# 19760) in series with an Rtx-1, 30 m, 0.53 mm ID, 5.0 μm (cat.# 10179) connected using a universal Press-Tight connector (cat. # 20401)

(conditions as per ASTM D6159-97)
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ASTM D6159-97

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