Pure Chromatography
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Diesel on Rxi-5HT

GC_PC1160
Column | Rxi-5HT, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13924) |
using Rxi guard column 2 m, 0.53 mm ID (cat.# 10054) | |
Sample | Diesel fuel #2 composite (cat.# 31258) |
Diluent: | Methylene chloride |
Conc.: | 50,000 µg/mL diluted to 500 ppm and spiked with C10 & C40 |
Injection | |
Inj. Vol.: | 1 µL cold on-column |
Temp. Program: | 53 °C to 300 °C at 10 °C/min (hold 20 min) |
Oven | |
Oven Temp.: | 50 °C to 300 °C at 10 °C/min (hold 20 min) |
Carrier Gas | H2, constant flow |
Linear Velocity: | 40 cm/sec @ 50 °C |
Dead Time: | 1.25 min @ 50 °C |
Detector | FID @ 330 °C |
Make-up Gas Flow Rate: | 30 mL/min |
Make-up Gas Type: | N2 |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
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