Pure Chromatography
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Diesel on Rtx-Mineral Oil

GC_PC1171
Column | Rtx-Mineral Oil, 15 m, 0.32 mm ID, 0.15 µm (cat.# 18074) |
using IP Deactivated Guard Column 2 m, 0.53 mm ID (cat.# 10047) | |
Sample | diesel fuel #2 composite (cat.# 31093) |
Diluent: | methylene chloride |
Conc.: | 5,000 µg/mL diluted to 500 μg/mL |
Injection | |
Inj. Vol.: | 0.5 µL cold on-column |
Temp. Program: | 53 °C to 300 °C at 10 °C/min (hold 20 min) |
Oven | |
Oven Temp.: | 50 °C to 300 °C at 10 °C/min (hold 20 min) |
Carrier Gas | H2, constant flow |
Linear Velocity: | 40 cm/sec @ 50 °C |
Dead Time: | 0.625 min @ 50 °C |
Detector | FID @ 330 °C |
Make-up Gas Flow Rate: | 30 mL/min |
Make-up Gas Type: | N2 |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
Notes | Black trace = diesel sample Red trace = C10-C30 standard |
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