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1,3-Butadiene on Rt-Alumina BOND/MAPD (Purity Analysis)

1,3-Butadiene on Rt-Alumina BOND/MAPD (Purity Analysis)

Peaks
1.Isobutane
2.n-Butane
3.Propadiene
4.trans-2-Butene
5.1-Butene
6.Isobutene
7.cis-2-Butene
8.Isopentane
9.n-Pentane
10.1,2-Butadiene
11.1,3-Butadiene
12.Methyl acetylene
image
GC_PC1211
ColumnRt-Alumina BOND/MAPD, 50 m, 0.53 mm ID, 10.0 µm (cat.# 19778)
SampleCrude 1,3-butadiene
Injection
Inj. Vol.:10 µL split
Liner:2.0 mm ID straight inlet liner (cat.# 20712)
Inj. Temp.:200 °C
Split Vent Flow Rate:100 mL/min
Oven
Oven Temp.:70 °C (hold 5 min) to 200 °C at 10 °C/min (hold 0 min)
Carrier GasHe, constant pressure (20 psi, 137.9 kPa)
DetectorFID @ 250 °C
Make-up Gas Flow Rate:30 mL/min
Make-up Gas Type:N2
Data Rate:20 Hz
InstrumentHP5890 GC
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