Pure Chromatography
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Aliphatic Amines on Stabilwax-DB

GC_PC1361
Column | Stabilwax-DB, 30 m, 0.53 mm ID, 1.00 µm (cat.# 10855) |
Sample | Custom aliphatic amines |
Diluent: | Methanol |
Conc.: | 1000 µg/mL |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 50:1) |
Liner: | Topaz 4.0 mm ID single taper inlet liner w/wool (cat.# 23303) |
Inj. Temp.: | 220 °C |
Oven | |
Oven Temp.: | 45 °C (hold 1 min) to 220 °C at 35 °C/min (hold 5 min) |
Carrier Gas | H2, constant flow |
Linear Velocity: | 40 cm/sec @ 45 °C |
Detector | FID @ 220 °C |
Make-up Gas Flow Rate: | 45 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 50 Hz |
Instrument | Agilent/HP6890 GC |
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