share:
delim
delim
Class 1 Residual Solvents for USP Water-Soluble Articles on Rxi-624Sil MS
This chromatogram may contain analytes that are synonyms of your search terms.

Class 1 Residual Solvents for USP <467> Water-Soluble Articles on Rxi-624Sil MS

PeakstR (min)Conc.
(µg/mL)
1.1,1-Dichloroethene3.5860.07
2.1,1,1-Trichloroethane8.5360.08
PeakstR (min)Conc.
(µg/mL)
3.Carbon tetrachloride9.0420.03
4.Benzene9.7870.02
5.1,2-Dichloroethane10.1120.04
* DMSO interference
image
GC_PH1160
ColumnRxi-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870)
SampleResidual Solvents - Class 1 (cat.# 36279)
Diluent:water
Injectionheadspace-loop split (split ratio 5:1)
Liner:1mm Split (cat.# 20972)
Headspace-Loop
Inj. Port Temp.:140 °C
Instrument:Tekmar HT3
Inj. Time:1 min
Transfer Line Temp.:110 °C
Valve Oven Temp.:110 °C
Sample Temp.:80 °C
Sample Equil. Time:60 min
Vial Pressure:10 psi
Pressurize Time:0.5 min
Pressure Equilibration Time:0.05 min
Loop Pressure:5 psi
Loop Fill Time:0.1 min
Oven
Oven Temp.:40 °C (hold 20 min) to 240 °C at 10 °C/min (hold 20 min)
Carrier GasHe, constant flow
Linear Velocity:35 cm/sec
Dead Time:1.45 min @ 40 °C
DetectorFID @ 250 °C
Data Rate:5 Hz
InstrumentAgilent/HP6890 GC
NotesColumns were run under identical conditions.
AcknowledgementTeledyne Tekmar
Download PDF

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us