Pure Chromatography
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USP <467> Residual Solvents Class 3 MIx A on Rxi-624Sil MS

GC_PH1178
Column | Rxi-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870) |
Sample | Residual Solvents Class 3 - Mix A (cat.# 36013) |
Conc.: | 5000 µg/mL split 100:1 |
Injection | headspace-loop split (split ratio 100:1) |
Liner: | Topaz 1 mm Split (cat.# 23333) |
Headspace-Loop | |
Inj. Port Temp.: | 200 °C |
Instrument: | Tekmar HT-3 |
Inj. Time: | 1.0 min |
Transfer Line Temp.: | 105 °C |
Valve Oven Temp.: | 105 °C |
Standby flow rate: | 50 mL/min |
Sample Temp.: | 80 °C |
Platen temp equil. time: | 80 min |
Sample Equil. Time: | 1.0 min |
Mixer time: | 5.0 min |
Mixing level: | 5 |
Mixer stabilize time: | 0.50 min |
Vial Pressure: | 10 psi |
Pressurize Time: | 5.0 min |
Pressure Equilibration Time: | 0.20 min |
Loop Pressure: | 5 psi |
Loop Fill Time: | 2.0 min |
Oven | |
Oven Temp.: | 35 °C (hold 3 min) to 60 °C at 24 °C/min to 80 °C at 3 °C/min to 280 °C at 25 °C/min |
Carrier Gas | He, constant flow |
Flow Rate: | 2.7 mL/min |
Linear Velocity: | 41 cm/sec |
Detector | FID @ 300 °C |
Make-up Gas Flow Rate: | 45 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
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