Pure Chromatography
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Fentanyl, Metabolite, and Analogues in Urine on Raptor Biphenyl by LC-MS/MS
| Peaks | tR (min) | Conc. (ng/mL) | Q1 | Q3 Quantifier | Q3 Qualifier | |
|---|---|---|---|---|---|---|
| 1. | Norfentanyl | 1.04 | 10 | 233.10 | 84.08 | 150.11 |
| 2. | Norfentanyl-d5 (IS) | 1.02 | 1 | 238.10 | 84.08 | - |
| 3. | Acetyl fentanyl | 1.48 | 10 | 323.29 | 188.18 | 105.10 |
| 4. | Acetyl fentanyl-13C6 | 1.48 | 1 | 329.22 | 188.22 | - |
| 5. | Fentanyl | 1.65 | 10 | 337.29 | 188.22 | 105.09 |
| 6. | Fentanyl-d5 (IS) | 1.64 | 1 | 342.35 | 188.22 | - |
| 7. | Sufentanil | 1.84 | 10 | 387.35 | 238.18 | 111.07 |
| 8. | Sufentanil-d5 (IS) | 1.83 | 1 | 392.29 | 238.18 | - |
LC_CF0591
| Column | Raptor Biphenyl (cat.# 9309552) | ||||||||||||||||||||
| Dimensions: | 50 mm x 2.1 mm ID | ||||||||||||||||||||
| Particle Size: | 5 µm | ||||||||||||||||||||
| Temp.: | 30 °C | ||||||||||||||||||||
| Sample | |||||||||||||||||||||
| Conc.: | A 10 ng/mL standard was prepared in urine. The internal standard was fortified to a final concentration of 1 ng/mL. An 80 μL aliquot of the 10 ng/mL urine standard was diluted with 320 μL of 70:30 water:methanol solution (5-fold dilution) prior to analysis. | ||||||||||||||||||||
| Inj. Vol.: | 5 µL | ||||||||||||||||||||
| Mobile Phase | |||||||||||||||||||||
| A: | 0.1% Formic acid in water | ||||||||||||||||||||
| B: | 0.1% Formic acid in methanol | ||||||||||||||||||||
| |||||||||||||||||||||
| Detector | MS/MS | ||||||||||||||||||||
| Ion Mode: | ESI+ | ||||||||||||||||||||
| Instrument | HPLC |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2020 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.