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22 Acylcarnitines and 13 Amino Acids in Solvent on Raptor HILIC-Si EXP Guard Cartridge Column by LC-MS/MS
Internal standard peaks not shown.
|Column||Raptor HILIC-Si EXP guard cartridge column (cat.# 9310A0252)|
|Dimensions:||5 mm x 2.1 mm ID|
|Particle Size:||2.7 µm|
|Diluent:||85:15 Acetonitrile:water (v/v)|
|Inj. Vol.:||2 µL|
|A:||30 mM Ammonium formate in water|
|Notes||A 100 ng/mL standard mix of 22 acylcarnitines and 13 amino acids was prepared in 85:15 acetonitrile:water (v/v) that was fortified with known concentrations of stable isotope-labeled internal standards. The solution was vortexed at 3000 rpm for 10 seconds to mix, and then the supernatant was injected for LC-MS/MS analysis.|
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