Pure Chromatography
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Pesticides on Pinnacle DB Aqueous C18
| Peaks | tR (min) | Polarity | Mol. Wt. | Transition 1 | |
|---|---|---|---|---|---|
| 1. | Methamidophos | 0.45 | positive | 141.13 | 142.0→94.0 |
| 2. | Acephate | 0.62 | positive | 183.17 | 184.0→142.8 |
| 3. | Bentazone | 0.77 | negative | 240.28 | 239.0→131.8 |
| 4. | Omethoate | 1.07 | positive | 213.14 | 214.0→124.9 |
| 5. | Bromoxynil | 1.32 | negative | 276.91 | 275.9→80.8 |
| 6. | Butoxycarboxin | 1.64 | positive | 222.27 | 223.1→86.1 |
| 7. | Aldicarb sulfoxide | 2.03 | positive | 206.26 | 207.1→132.1 |
| 8. | Methomyl | 2.08 | positive | 162.21 | 163.1→88.1 |
| 9. | Ioxynil | 2.46 | negative | 370.92 | 369.8→126.7 |
| 10. | Thiamethoxam | 2.7 | positive | 291.7 | 292.0→211.0 |
| 11. | Monocrotophos | 2.73 | positive | 223.17 | 224.1→127.0 |
| 12. | Dimethoate | 2.9 | positive | 229.26 | 230.1→199.0 |
| 13. | Fenuron | 3.1 | positive | 164.21 | 165.1→72.1 |
| 14. | Dioxacarb | 3.12 | positive | 223.23 | 224.0→123.0 |
| 15. | Dicrotophos | 3.28 | positive | 237.19 | 238.0→112.0 |
| 16. | Vamidothion | 3.45 | positive | 287.34 | 288.0→146.0 |
| 17. | Carbendazim | 3.73 | positive | 191.19 | 192.0→160.0 |
| 18. | Aldicarb | 3.73 | positive | 190.27 | 208.1→116.0 |
| 19. | Formetanate | 3.74 | positive | 221.26 | 222.1→165.2 |
| 20. | Acetamiprid | 3.95 | positive | 222.67 | 223.1→126.1 |
| 21. | Carbetamide | 3.99 | positive | 236.27 | 237.0→192.0 |
| 22. | Oxamyl | 3.99 | positive | 219.26 | 237.1→72.2 |
| 23. | Aminocarb | 4.11, 4.44 | positive | 208.26 | 209.2→137.1 |
| 24. | Propoxur | 4.15 | positive | 209.24 | 210.1→111.0 |
| 25. | Oxadixyl | 4.21 | positive | 278.31 | 279.0→219.0 |
| 26. | Bendiocarb | 4.24 | positive | 223.23 | 224.1→109.1 |
| 27. | Thiacloprid | 4.25 | positive | 252.71 | 253.2→126.1 |
| 28. | Thiophanate methyl | 4.3 | positive | 342.4 | 343.0→151.0 |
| 29. | Methabenzthiazuron | 4.31 | positive | 221.28 | 222.0→165.1 |
| 30. | Tricyclazole | 4.35 | positive | 189.23 | 190.0→163.0 |
| 31. | Pyracarbolid | 4.38 | positive | 217.27 | 218.2→125.0 |
| 32. | Propamocarb | 4.41 | positive | 188.27 | 189.2→102.2 |
| 33. | Carboxin | 4.51 | positive | 235.3 | 236.0→143.0 |
| 34. | Ethiofencarb | 4.52 | positive | 225.31 | 226.1→106.9 |
| 35. | Carbaryl | 4.58 | positive | 201.22 | 202.1→145.1 |
| 36. | Thiabendazole | 4.6 | positive | 201.25 | 202.0→175.0 |
| 37. | Carbanilide | 4.6 | positive | 212.25 | 213.1→94.0 |
| 38. | Clethodim | 4.61 | positive | 359.91 | 360.0→164.0 |
| 39. | Tebuthiuron | 4.68 | positive | 228.32 | 229.2→172.4 |
| 40. | Fluometuron | 4.75 | positive | 232.21 | 233.1→72.0 |
| 41. | Metobromuron | 4.82 | positive | 259.1 | 259.0→170.2 |
| 42. | Flutriafol | 4.84 | positive | 301.3 | 302.0→123.0 |
| 43. | Chlortoluron | 4.92 | positive | 212.68 | 213.1→72.2 |
| 44. | Simetryn | 4.96 | positive | 213.31 | 214.0→124.0 |
| 45. | Pirimicarb | 4.97 | positive | 238.29 | 239.2→72.1 |
| 46. | Forchlorfenuron | 5.04 | positive | 247.68 | 248.0→129.1 |
| 47. | Siduron | 5.09 | positive | 232.32 | 233.3→137.2 |
| 48. | Ethofumesate | 5.11 | positive | 286.35 | 304.0→121.0 |
| 49. | Cycluron | 5.13 | positive | 198.31 | 199.1→89.1 |
| 50. | Diuron | 5.13 | positive | 233.1 | 233.1→72.0 |
| 51. | Diethofencarb | 5.15 | positive | 267.33 | 268.0→226.0 |
| 52. | Furalaxyl | 5.18 | positive | 301.34 | 302.2→95.0 |
| 53. | Methiocarb | 5.24 | positive | 225.31 | 226.1→169.2 |
| 54. | Secbumeton | 5.24 | positive | 225.29 | 226.2→169.9 |
| 55. | Terbumeton | 5.25 | positive | 225.29 | 226.2→169.9 |
| 56. | Prometon | 5.26 | positive | 225.29 | 226.2→142.3 |
| 57. | Paclobutrazol | 5.26 | positive | 293.8 | 294.0→70.0 |
| 58. | Promecarb | 5.27 | positive | 207.27 | 208.2→109.2 |
| 59. | Dimoxystrobin | 5.27 | positive | 326.39 | 327.1→205.0 |
| 60. | Ametryn | 5.29 | positive | 227.33 | 228.2→186.2 |
| 61. | Methoprotryne | 5.32 | positive | 271.39 | 272.2→240.2 |
| 62. | Triadimefon | 5.32 | positive | 293.75 | 294.0→197.0 |
| 63. | Mexacarbate | 5.34 | positive | 222.28 | 223.2→166.2 |
| 64. | Fludioxonil | 5.34 | negative | 248.19 | 247.0→179.9 |
| 65. | Boscalid | 5.36 | negative | 343.21 | 343.0→307.0 |
| 66. | Azoxystrobin | 5.36 | positive | 403.3 | 404.1→372.1 |
| 67. | Methoxyfenozide | 5.38 | positive | 368.47 | 369.0→149.0 |
| 68. | Cyproconazole | 5.39 | positive | 291.78 | 292.2→70.2 |
| 69. | Prothioconazole | 5.41 | negative | 344.26 | 341.9→305.8 |
| 70. | Flufenacet | 5.46 | positive | 363.34 | 364.0→152.0 |
| 71. | Butafenacil | 5.47 | positive | 474.82 | 492.2→331.1 |
| 72. | Myclobutanil | 5.51 | positive | 288.78 | 289.0→70.0 |
| 73. | Dimethomorph | 5.52,5.54 | positive | 387.86 | 388.0→301.0 |
| 74. | Bromuconazole 47 | 5.54 | positive | 377.06 | 378.0→159.0 |
| 75. | Prometryn | 5.55 | positive | 241.36 | 242.2→158.1 |
| 76. | Fipronil | 5.56 | negative | 437.15 | 434.9→329.8 |
| 77. | Triticonazole | 5.58 | positive | 317.81 | 318.0→70.0 |
| 78. | Tetraconazole | 5.6 | positive | 372.12 | 372.0→159.0 |
| 79. | Uniconazole | 5.62 | positive | 291.78 | 292.2→70.2 |
| 80. | Fluoxastrobin | 5.62 | positive | 458.83 | 459.2→427.2 |
| 81. | Cyazofamid | 5.63 | positive | 324.78 | 325.0→108.0 |
| 82. | Terbutryn | 5.65 | positive | 241.36 | 242.2→186.0 |
| 83. | Tebufenozide | 5.65 | positive | 352.47 | 353.1→133.1 |
| 84. | Chloroxuron | 5.67 | positive | 290.75 | 291.0→72.0 |
| 85. | Picoxystrobin | 5.67 | positive | 367.25 | 368.0→145.0 |
| 86. | Carfentrazone ethyl | 5.69 | positive | 412.17 | 412.0→346.0 |
| 87. | Diclobutrazol | 5.71 | positive | 328.21 | 328.0→70.0 |
| 88. | Fenoxycarb | 5.72 | positive | 301.34 | 302.0→88.1 |
| 89. | Diflubenzuron | 5.72 | positive | 310.67 | 311.2→158.1 |
| 90. | Neburon | 5.74 | positive | 275.18 | 275.0→88.0 |
| 91. | Flusilazole | 5.76 | positive | 315.4 | 316.0→247.0 |
| 92. | Epoxiconazole | 5.76 | positive | 329.76 | 330.0→121.0 |
| 93. | Fenbuconazole | 5.76 | positive | 336.82 | 337.0→125.0 |
| 94. | Bupirimate | 5.77 | positive | 316.41 | 317.0→166.0 |
| 95. | Zoxamide | 5.77 | positive | 336.54 | 336.2→187.1 |
| 96. | Rotenone | 5.79 | positive | 394.42 | 395.0→213.0 |
| 97. | Benalaxyl | 5.83 | positive | 325.41 | 326.0→148.0 |
| 98. | Tebuconazole | 5.84 | positive | 307.82 | 308.0→70.0 |
| 99. | Penconazole | 5.93 | positive | 284.19 | 284.0→159.0 |
| 100. | Cyprodinil | 5.96 | positive | 225.29 | 226.0→93.0 |
| 101. | Propiconazole | 5.96 | positive | 342.22 | 342.0→159.0 |
| 102. | Alanycarb | 5.98 | positive | 399.52 | 400.1→238.2 |
| 103. | Triflumuron | 5.99 | positive | 358.68 | 359.1→156.1 |
| 104. | Thiobencarb | 6 | positive | 257.78 | 258.1→125.0 |
| 105. | Pyraclostrobin | 6 | positive | 387.83 | 388.0→194.0 |
| 106. | Benzoximate | 6.01 | positive | 363.8 | 364.0→199.0 |
| 107. | Pinoxaden | 6.01 | positive | 400.52 | 401.3→317.2 |
| 108. | Clofentezine | 6.11 | positive | 303.15 | 303.0→138.0 |
| 109. | Trifloxystrobin | 6.12 | positive | 408.38 | 409.2→186.0 |
| 110. | Prochloraz | 6.21 | positive | 376.67 | 376.0→308.0 |
| 111. | Difenoconazole | 6.29 | positive | 406.28 | 406.0→251.0 |
| 112. | Benfuracarb | 6.29 | positive | 410.53 | 411.2→195.1 |
| 113. | Triflumizole | 6.38 | positive | 345.75 | 346.1→278.1 |
| 114. | Buprofezin | 6.4 | positive | 305.44 | 306.0→201.0 |
| 115. | Piperonyl butoxide | 6.42 | positive | 338.45 | 356.2→177.2 |
| 116. | Pyriproxyfen | 6.52 | positive | 321.28 | 322.0→96.0 |
| 117. | Propargite | 6.68 | positive | 350.48 | 368.0→231.0 |
| 118. | Etoxazole | 6.87 | positive | 359.42 | 360.1→141.0 |
| 119. | Amitraz | 6.89 | positive | 293.41 | 294.2→163.3 |
| 120. | Noviflumuron | 7.08 | negative | 529.1 | 527.1→343.8 |
| 121. | Pyridaben | 7.18 | positive | 364.94 | 365.0→147.0 |
| 122. | Fenpyroximate | 7.2 | positive | 421.5 | 422.0→366.0 |
| 123. | Fenpropimorph | 7.38 | positive | 303.49 | 304.0→147.0 |
| 124. | Spiroxamine | 7.63,7.81 | positive | 297.48 | 298.0→144.0 |
| 125. | Spinosyn A | 8.37 | positive | 731.97 | 732.6→142.2 |
LC_FF0479A
| Column | Pinnacle DB Aqueous C18 (cat.# 9418252) | ||||||||||||
| Dimensions: | 50 mm x 2.1 mm ID | ||||||||||||
| Particle Size: | 1.9 µm | ||||||||||||
| Pore Size: | 140 Å | ||||||||||||
| Temp.: | 35 °C | ||||||||||||
| Sample | multicomponent pesticide standard | ||||||||||||
| Diluent: | water | ||||||||||||
| Conc.: | 33.3 ppb each pesticide | ||||||||||||
| Inj. Vol.: | 5 µL | ||||||||||||
| Mobile Phase | |||||||||||||
| A: | 10 mM NH4OAc in water | ||||||||||||
| B: | 10 mM NH4OAc in methanol | ||||||||||||
| |||||||||||||
| Flow: | 0.60 mL/min | ||||||||||||
| Max Pressure: | ~517 bar | ||||||||||||
| Detector | Applied Biosystems/MDS Sciex LC/MS/MS | ||||||||||||
| Model #: | 4000 QTRAP LC-MS/MS system | ||||||||||||
| Ion Source: | TurboIonSpray® | ||||||||||||
| Ion Spray Voltage: | 5 kV | ||||||||||||
| Gas 1: | 40 psi (275.8 kPa) | ||||||||||||
| Gas 2: | 60 psi (413.7 kPa) | ||||||||||||
| Source Temp.: | 500 °C | ||||||||||||
| Instrument | Shimadzu UFLCXR |
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Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823
Copyright © 2019 Restek Corporation. All rights reserved.
A Company of Owners
Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.