Pure Chromatography
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LC Multiresidue Pesticide Standard #4 on Raptor ARC-18 by LC-MS/MS
| Peaks | tR (min) | Precursor Ion | Product Ion 1 | Product Ion 2 | |
|---|---|---|---|---|---|
| 1. | Cyromazine | 1.07 | 167.0 | 85.0 | 108.1 |
| 2. | Pymetrozine | 1.35 | 218.0 | 105.0 | 79.0 |
| 3. | Dinotefuran | 1.63 | 203.0 | 129.0 | 157.0 |
| 4. | Nitenpyram | 1.68 | 271.1 | 125.9 | 224.9 |
| 5. | Flonicamid | 1.89 | 230.0 | 203.1 | 174.1 |
| 6. | Imidacloprid | 2.19 | 256.1 | 175.1 | 209.1 |
| 7. | Acetamiprid | 2.40 | 223.0 | 126.0 | 56.1 |
| 8. | Cymoxanil | 2.47 | 199.0 | 128.0 | 111.0 |
| 9. | Oxadixyl | 2.77 | 279.0 | 219.0 | 132.0 |
| 10. | Carbetamide | 2.79 | 237.0 | 118.0 | 192.0 |
| 11. | Secbumeton | 2.93 | 226.2 | 100.2 | 170.2 |
| 12. | Prometon | 2.93 | 226.0 | 86.3 | 184.3 |
| 13. | Terbumeton | 2.97 | 226.1 | 114.1 | 170.1 |
| 14. | Imazalil | 2.97 | 297.0 | 159.0 | 69.0 |
| 15. | Pyracarbolid | 3.04 | 218.1 | 125.1 | 97.1 |
| 16. | Ametryn | 3.22 | 228.1 | 68.1 | 186.1 |
| 17. | Pyrimethanil | 3.51 | 200.0 | 107.0 | 82.0 |
| 18. | Spiroxamine isomer 1 | 3.56 | 298.0 | 144.0 | 100.0 |
| 19. | Metalaxyl | 3.56 | 280.1 | 220.1 | 192.1 |
| 20. | Spiroxamine isomer 2 | 3.62 | 298.0 | 144.0 | 100.0 |
| 21. | Chlorantraniliprole | 3.66 | 483.9 | 286.0 | 453.0 |
| 22. | Azoxystrobin | 3.92 | 404.1 | 372.0 | 329.0 |
| 23. | Furalaxyl | 3.96 | 302.1 | 270.1 | 242.2 |
| 24. | Fludioxonil | 3.97 | 249.1 | 229.1 | 158.1 |
| 25. | Halofenozide | 3.98 | 331.1 | 104.9 | 275.0 |
| 26. | Boscalid | 4.06 | 342.9 | 307.0 | 139.9 |
| 27. | Mandipropamid | 4.08 | 412.3 | 328.2 | 356.2 |
| 28. | Flutolanil | 4.10 | 324.1 | 262.1 | 65.0 |
| 29. | Mepronil | 4.20 | 270.1 | 91.0 | 119.0 |
| 30. | Myclobutanil | 4.25 | 289.1 | 125.1 | 70.2 |
| 31. | Methoxyfenozide | 4.29 | 369.1 | 149.1 | 313.2 |
| 32. | Triadimefon | 4.33 | 294.1 | 197.2 | 69.3 |
| 33. | Cyprodinil | 4.34 | 226.0 | 93.0 | 108.0 |
| 34. | Mepanipyrim | 4.40 | 224.1 | 106.0 | 77.0 |
| 35. | Fenhexamid | 4.46 | 302.1 | 97.2 | 55.3 |
| 36. | Fluoxastrobin | 4.46 | 459.0 | 427.0 | 188.0 |
| 37. | Butafenacil | 4.48 | 492.0 | 180.0 | 331.0 |
| 38. | Picoxystrobin | 4.78 | 368.0 | 145.1 | 205.1 |
| 39. | Rotenone | 4.83 | 395.0 | 213.1 | 192.1 |
| 40. | Tebufenozide | 4.86 | 353.1 | 133.0 | 297.1 |
| 41. | Dimoxystrobin | 4.87 | 327.1 | 116.1 | 205.2 |
| 42. | Carfentrazone ethyl | 4.89 | 412.0 | 346.0 | 266.0 |
| 43. | Kresoxim-methyl | 4.90 | 314.1 | 206.0 | 116.0 |
| 44. | Zoxamide | 5.06 | 336.0 | 187.1 | 159.0 |
| 45. | Famoxadone | 5.09 | 392.2 | 331.1 | 238.0 |
| 46. | Prochloraz | 5.14 | 376.0 | 308.0 | 70.1 |
| 47. | Benalaxyl | 5.15 | 326.1 | 148.0 | 91.0 |
| 48. | Clofentezine | 5.21 | 303.0 | 138.0 | 102.0 |
| 49. | Benzoximate | 5.28 | 364.0 | 199.1 | 105.0 |
| 50. | Trifloxystrobin | 5.50 | 409.0 | 186.0 | 145.0 |
| 51. | Fluazinam | 5.77 | 464.8 | 373.0 | 338.1 |
| 52. | Metaflumizone | 5.79 | 507.0 | 287.2 | 267.1 |
| 53. | Tebufenpyrad | 5.85 | 334.0 | 117.0 | 145.0 |
| 54. | Pyriproxifen | 5.91 | 322.1 | 96.0 | 227.1 |
| 55. | Piperonyl butoxide | 5.93 | 356.3 | 176.9 | 119.0 |
| 56. | Quinoxyfen | 6.03 | 308.0 | 197.0 | 161.9 |
| 57. | Amitraz | 6.14 | 294.0 | 163.0 | 122.0 |
| 58. | Fenpyroximate | 6.36 | 422.2 | 138.1 | 366.1 |
| 59. | Abamectin B1b | 6.47 | 876.6 | 553.4 | 291.0 |
| 60. | Eprinomectin | 6.53 | 914.6 | 186.0 | 154.0 |
| 61. | Abamectin B1a | 6.61 | 890.5 | 305.2 | 567.3 |
| 62. | Fenazaquin | 6.68 | 307.2 | 161.0 | 57.2 |
| 63. | Doramectin | 6.81 | 916.6 | 331.2 | 593.4 |
| 64. | Moxidectin | 6.81 | 640.5 | 498.3 | 528.4 |
| 65. | Ivermectin | 7.00 | 892.6 | 569.4 | 551.4 |
Isomers are numbered sequentially based on elution order.
LC_FF0546
| Column | Raptor ARC-18 (cat.# 9314A12) | ||||||||||||||||||||||||||||||||
| Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||||||||||
| Particle Size: | 2.7 µm | ||||||||||||||||||||||||||||||||
| Temp.: | 50 °C | ||||||||||||||||||||||||||||||||
| Sample | LC multiresidue pesticide standard #4 (cat.# 31975) | ||||||||||||||||||||||||||||||||
| Diluent: | Water | ||||||||||||||||||||||||||||||||
| Conc.: | 20 ng/mL | ||||||||||||||||||||||||||||||||
| Inj. Vol.: | 5 µL | ||||||||||||||||||||||||||||||||
| Mobile Phase | |||||||||||||||||||||||||||||||||
| A: | Water + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
| B: | Methanol + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
| |||||||||||||||||||||||||||||||||
| Detector | Waters Xevo TQ-S | ||||||||||||||||||||||||||||||||
| Ion Source: | Waters Zspray™ ESI | ||||||||||||||||||||||||||||||||
| Ion Mode: | ESI+ | ||||||||||||||||||||||||||||||||
| Mode: | MRM | ||||||||||||||||||||||||||||||||
| Instrument | Waters | ||||||||||||||||||||||||||||||||
| Notes | Autosampler Temp. = 5 °C |
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Copyright © 2020 Restek Corporation. All rights reserved.
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Cookies allow for a variety of features that make your visit to Restek more enjoyable. By using this website, you agree to the use of cookies in accordance with our guidelines. For more information, see our privacy policy.