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Mass APH on Rxi-1ms

ColumnRxi-1ms, 60 m, 0.32 mm ID, 1.00 µm (cat.# 13357)
Injectionsplitless
Oven
Oven Temp.:35 °C (hold 5 min) to 220 °C at 7 °C/min (hold 2 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:240 °C
Analyzer Type:Quadrupole
Source Temp.:230 °C
Quad Temp.:150 °C
Solvent Delay Time:4.0 min
Ionization Mode:EI
Scan Range:35-250 amu
PreconcentratorEntech 7100
InstrumentHP6890 GC & 5973 MSD
AcknowledgementCourtesy of Mass DEP, Northeast Region