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Amines/Alcohols/Chlorides on Stabilwax

GC_CH00307
Peaks
1.n-Octyl,N,N-dimethylamine
2.n-Octyl chloride
3.n-Decyl,N,N-dimethylamine
4.n-Decyl chloride
5.n-Octyl alcohol
6.n-Dodecyl,N,N-dimethylamine
7.n-Dodecyl chloride
8.n-Decyl alcohol
Peaks
9.n-Tetradecyl,N,N-dimethylamine
10.n-Tetradecyl chloride
11.n-Dodecyl alcohol
12.n-Hexadecyl,N,N-dimethylamine
13.n-Hexadecyl chloride
14.n-Tetradecyl alcohol
15.n-Octadecyl,N,N-dimethylamine
16.n-Hexadecyl alcohol
17.n-Octadecyl alcohol
ColumnStabilwax, 30 m, 0.53 mm ID, 0.25 µm (cat.# 10625)
Injection
Inj. Vol.:0.5 µL split (split ratio 40:1)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 250 °C at 8 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:5.2 mL/min
Linear Velocity:40 cm/sec
DetectorFID @ 250 °C
NotesFID sensitivity: 128 x 10-11 AFS